1-Octanesulfonamide

Base Information

• Chemical Name: 1-Octanesulfonamide
• CAS No.: 65501-71-5
• Molecular Formula: C8H19NO2S
• Molecular Weight: 193.31
• Hs Code.: 2935009090
• Mol file: 65501-71-5.mol

Synonyms:AmbkkkkK564;octanesulfonamide;n-octylsulfonamide;n-octanesulfonamide;propyl Pentanesulfonamide;1-octanesulfonamide;Octan-1-sulfonsaeure-amid;

Chemical Property of 1-Octanesulfonamide

Chemical Property:

• Vapor Pressure: 0.000917mmHg at 25°C
• Boiling Point: 303.7°Cat760mmHg
• PKA: 10.86±0.60(Predicted)
• Flash Point: 137.5°C
• PSA: 68.54000
• Density: 1.043g/cm³
• LogP: 3.41650

Purity/Quality:

99.3% ^*data from raw suppliers

1-OCTANESULFONAMIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-Octanesulfonamide

There total 8 articles about 1-Octanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

N-isopropyl octylsulfonamide → 1-octanesulfonamide (65501-71-5)

Guidance literature:

With chromium(III) acetate hydroxide; periodic acid; In acetonitrile; at 20 ℃; for 7h;

DOI:10.1055/s-2004-830851

Reference yield: 88.0%

octane-1-sulfonyl chloride (7795-95-1) → 1-octanesulfonamide (65501-71-5)

Guidance literature:

With ammonia; In ethyl acetate; at 0 - 20 ℃; for 0.75h;

DOI:10.1016/j.ejmech.2009.11.052

Reference yield: 56.0%

octane-1-sulfonyl azide (98487-74-2) + allytriphenyltin (76-63-1) → 1-octanesulfonamide (65501-71-5) + 1-(allylsulfonyl)octane + Octane-1-sulfonic acid allylamide

Guidance literature:

With 2,2'-azobis(isobutyronitrile); In benzene; for 3h; Heating;

DOI:10.1039/p19960001493

upstream raw materials:

octane-1-sulfonyl chloride

octane-1-sulfonyl azide

allytriphenyltin

1-bromo-octane

Downstream raw materials:

(Z)-N-(2-cyano-3-phenylprop-2-en-1-yl)-octanesulfonamide

N-phenyloctane-1-sulfonamide

(2R)-N-benzyloxycarbonyl(octanesulfonyl pyrrolidine-2-carboxamide)

[2-(Octane-1-sulfonylamino)-2-oxo-ethyl]-carbamic acid benzyl ester

Refernces

• 1、 Vidigal, Antonio E.C.,Rubinger, Mayura M.M.,de Queiroz, Luan F.,da Silva, Lucas F.,Zambolim, Laércio,Guilardi, Silvana,Souza, Rafael A.C.,Ellena, Javier,Wetler, Emiliana B.,Oliveira, Marcelo R.L.. "Nickel complexes with phosphines and N-R-sulfonyldithiocarbimates ligands: New antifungals for the control of Hemileia vastatrix and Phakopsora pachyrhizi". . p. 724 - 732. Retrieved 2018/12/11.
• 2、 Tavares, Eder C.,Rubinger, Mayura M.M.,Zacchi, Carlos H.C.,Silva, Simone A.,Oliveira, Marcelo R.L.,Guilardi, Silvana,Alcantara, Ant?nio F. De C.,Piló-Veloso, Dorila,Zambolim, Laércio. "Synthesis, characterization, and antifungal activity of novel (Z)-N-(2-cyano-3-phenylprop-2-en-1-yl)-alkyl/aryl-sulfonamides derived from a Morita-Baylis-Hillman adduct". . p. 43 - 51. Retrieved 2014/04/17.