10-Methylanthracene-9-carbaldehyde

Base Information

• Chemical Name: 10-Methylanthracene-9-carbaldehyde
• CAS No.: 7072-00-6
• Molecular Formula: C16H12 O
• Molecular Weight: 220.271
• Hs Code.: 2912299000
• European Community (EC) Number: 230-366-9
• NSC Number: 97075
• DSSTox Substance ID: DTXSID40220982
• Nikkaji Number: J149.919J
• Wikidata: Q83098522
• Mol file: 7072-00-6.mol

Synonyms:10-Methylanthracene-9-carbaldehyde;7072-00-6;10-Methylanthracene-9-carboxaldehyde;9-Anthracenecarboxaldehyde, 10-methyl-;EINECS 230-366-9;9-METHYL-10-ANTHRALDEHYDE;NSC97075;10-methyl 9-anthraldehyde;SCHEMBL4164444;DTXSID40220982;10-Methyl-9-anthracenecarbaldehyde;NSC 97075;NSC-97075;10-Methyl-9-anthracenecarbaldehyde #;AKOS015913235;10-Methylanthracene-9-carboxaldehyde, 96%;CS-0108727;FT-0746975;E79071

Chemical Property of 10-Methylanthracene-9-carbaldehyde

Chemical Property:

• Vapor Pressure: 3.24E-07mmHg at 25°C
• Melting Point: 169-171.5 °C(lit.)
• Refractive Index: 1.5800 (estimate)
• Boiling Point: 418.6°C at 760 mmHg
• Flash Point: 269.2°C
• PSA: 17.07000
• Density: 1.186g/cm³
• LogP: 4.11390
• XLogP3: 4.2
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 1
• Exact Mass: 220.088815002
• Heavy Atom Count: 17
• Complexity: 261

Purity/Quality:

98%,99%, ^*data from raw suppliers

10-Methylanthracene-9-carboxaldehyde 96% ^*data from reagent suppliers

Safty Information:

• Safety Statements: S24/25:Avoid contact with skin and eyes.

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Canonical SMILES: CC1=C2C=CC=CC2=C(C3=CC=CC=C13)C=O

Technology Process of 10-Methylanthracene-9-carbaldehyde

There total 32 articles about 10-Methylanthracene-9-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

triformylamine (25891-31-0) + 9-methylanthracene (779-02-2) → 10-methyl-9-anthraldehyde (7072-00-6)

Guidance literature:

With aluminium trichloride; In chlorobenzene; at 3 - 20 ℃; for 16h;

Reference yield: 56.0%

9,10-dimethylanthracene (781-43-1) → 9,10-diformylanthracene (7044-91-9) + 10-methyl-9-anthraldehyde (7072-00-6)

Guidance literature:

With benzeneseleninic anhydride; In chlorobenzene; at 110 ℃; for 0.583333h;

Reference yield: 52.0%

9-methylanthracene (779-02-2) + N,N-dimethyl-formamide (68-12-2,33513-42-7) → 10-methyl-9-anthraldehyde (7072-00-6)

Guidance literature:

With trichlorophosphate; In 1,2-dichloro-benzene; at 100 - 110 ℃;

DOI:10.1016/j.molstruc.2020.128578

upstream raw materials:

9-methylanthracene

N-methyl-N-phenylformamide

9,10-dimethylanthracene

iodoxybenzene

Downstream raw materials:

10-hydroxy-10-methylanthracen-9(10H)-one

9,10-phenanthrenequinone

Refernces

• 1、 Chari, Rama,Jayabalan, J.,Saha, Amrita,Singh, Asha. "Unraveling relation between nonlinear absorption and structure of push pull ornamented anthracenyl chalcone derivatives". . . Retrieved 2020/06/27.
• 2、 -. "Process for nucleophilic fluoroalkylation of aldehydes". . . Retrieved 2008/06/13.