3-Chlorooxolane-2,5-dione

Base Information

• Chemical Name: 3-Chlorooxolane-2,5-dione
• CAS No.: 1192-71-8
• Molecular Formula: C4H3ClO3
• Molecular Weight: 134.519
• Hs Code.: 2917190090
• DSSTox Substance ID: DTXSID30521091
• Nikkaji Number: J150.157G
• Mol file: 1192-71-8.mol

Synonyms:3-Chlorooxolane-2,5-dione;1192-71-8;2,5-Furandione, 3-chlorodihydro-;3-Chloro-3,4-dihydro-2,5-furandione;3-Chloro-dihydrofuran-2,5-dione;chlorosuccinic anhydride;SCHEMBL1995961;3-Chlorodihydrofuran-2,5-dione;DTXSID30521091;A902068

Chemical Property of 3-Chlorooxolane-2,5-dione

Chemical Property:

• Melting Point: 43.5-44 °C(Solv: ethyl ether (60-29-7))
• Boiling Point: 68-80 °C(Press: 0.1 Torr)
• PSA: 43.37000
• Density: 1.51±0.1 g/cm3(Predicted)
• LogP: 0.06730
• XLogP3: 0.3
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 0
• Exact Mass: 133.9770716
• Heavy Atom Count: 8
• Complexity: 142

Purity/Quality:

98%,99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1C(C(=O)OC1=O)Cl

Technology Process of 3-Chlorooxolane-2,5-dione

There total 4 articles about 3-Chlorooxolane-2,5-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

acetyl chloride (75-36-5) + (2E)-but-2-enedioic acid (110-17-8,26099-09-2) → maleic anhydride (108-31-6) + (S)-chlorosuccinic anhydride (1192-71-8)

Guidance literature:

With acetic acid; anhydride of/the/ inactive chlorosuccinic acid; im Druckrohr;

Reference yield:

acetic acid (64-19-7,77671-22-8) + acetyl chloride (75-36-5) + (2E)-but-2-enedioic acid (110-17-8,26099-09-2) → maleic anhydride (108-31-6) + (S)-chlorosuccinic anhydride (1192-71-8)

Guidance literature:

at 100 ℃;

Reference yield:

(2E)-but-2-enedioic acid (110-17-8,26099-09-2) → maleic acid (110-16-7,26099-09-2) + (S)-chlorosuccinic anhydride (1192-71-8)

Guidance literature:

With acetyl chloride; at 140 ℃; entsteht das Anhydrid;

upstream raw materials:

acetic acid

acetyl chloride

(2E)-but-2-enedioic acid

fumaryl dichloride

Downstream raw materials:

maleic anhydride

maleic acid

L-carnitine

1-benzyl 2-chlorosuccimic dicyclohexylammonium