2-BroMo-3,5-diMethylphenol

Base Information

• Chemical Name: 2-BroMo-3,5-diMethylphenol
• CAS No.: 125237-08-3
• Molecular Formula: C8H9BrO
• Molecular Weight: 201.063
• Hs Code.: 2908190090
• Mol file: 125237-08-3.mol

Synonyms:4-Brom-5-oxy-m-xylol;2-bromo-3,5-dimethyl-phenol;2-Brom-symm.-m-xylenol;2-Brom-3,5-dimethylphenol;2-Brom-3,5-xylenol;2-Brom-3,5-dimethyl-phenol;

Chemical Property of 2-BroMo-3,5-diMethylphenol

Chemical Property:

• PSA: 20.23000
• LogP: 2.77150
• Storage Temp.: 2-8°C

Purity/Quality:

99%, ^*data from raw suppliers

2-Bromo-3,5-dimethylphenol 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-BroMo-3,5-diMethylphenol

There total 4 articles about 2-BroMo-3,5-diMethylphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

3,5-Dimethylphenol (108-68-9,50356-23-5) → 2-bromo-3,5-dimethylphenol (125237-08-3)

Guidance literature:

With N-Bromosuccinimide; In carbon disulfide; at 0 - 20 ℃; for 2h;

Reference yield:

3,5-Dimethylphenol (108-68-9,50356-23-5) → 4-bromo-3,5-dimethylphenol (7463-51-6) + 2-bromo-3,5-dimethylphenol (125237-08-3)

Guidance literature:

With sulfuric acid; dihydrogen peroxide; cetyltrimethylammonim bromide; sodium dodecyl-sulfate; sodium bromide; for 2h; Micellar solution;

DOI:10.1007/s00706-011-0677-1

Reference yield:

→ 2-bromo-3,5-dimethylphenol (125237-08-3)

Guidance literature:

With copper(I) bromide;

upstream raw materials:

3,5-Dimethylphenol

Refernces

• 1、 Samant, Bhupesh S.,Bhagwat, Sunil S.. "Selectivity enhancement of aromatic halogenation reactions at the micellar interface: Effect of highly ionic media". scheme or table. p. 1039 - 1044. Retrieved 2012/10/18.
• 2、 -. "Benzofuran derivatives". Page/Page column 66. . Retrieved 2010/09/18.