Tetracosanoic acid, 24-[(1-oxo-9,12-octadecadienyl)oxy]-, 4-nitrophenyl ester, (Z,Z)-

Base Information

• Chemical Name: Tetracosanoic acid, 24-[(1-oxo-9,12-octadecadienyl)oxy]-, 4-nitrophenyl ester, (Z,Z)-
• CAS No.: 131105-35-6
• Molecular Formula: C₄₈H₈₁NO₆
• Molecular Weight: 768.174
• Mol file: 131105-35-6.mol

Synonyms:

Chemical Property of Tetracosanoic acid, 24-[(1-oxo-9,12-octadecadienyl)oxy]-, 4-nitrophenyl ester, (Z,Z)-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Tetracosanoic acid, 24-[(1-oxo-9,12-octadecadienyl)oxy]-, 4-nitrophenyl ester, (Z,Z)-

There total 10 articles about Tetracosanoic acid, 24-[(1-oxo-9,12-octadecadienyl)oxy]-, 4-nitrophenyl ester, (Z,Z)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

linoleyl chloride (7459-33-8) → p-nitrophenyl 24-linoleoxytetracosanoate (131105-35-6)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine / CHCl₃ / 5 h / Ambient temperature

2: pyridine / 2 h / Ambient temperature

With pyridine; In chloroform;

Reference yield:

1,13-tridecanediol (13362-52-2) → p-nitrophenyl 24-linoleoxytetracosanoate (131105-35-6)

Guidance literature:

Multi-step reaction with 7 steps

1: 73 percent / 48percent hydrobromic acid / benzene / 36 h / Heating

2: 98 percent / pyridinium p-toluenesulfonate / CH₂Cl₂ / 4 h / Ambient temperature

3: 1) magnesium, 2) Li₂CuCl₄ / 1) THF, 2) room temperature, 3 h

4: NaOH / ethanol / 2 h / Heating

5: 2 N HCl / ethanol / 1 h / Heating

6: pyridine / CHCl₃ / 5 h / Ambient temperature

7: pyridine / 2 h / Ambient temperature

With pyridine; hydrogenchloride; sodium hydroxide; dilithium tetrachlorocuprate; hydrogen bromide; pyridinium p-toluenesulfonate; magnesium; In ethanol; dichloromethane; chloroform; benzene;

Reference yield:

13-bromo-1-tridecylalcohol (116754-58-6) → p-nitrophenyl 24-linoleoxytetracosanoate (131105-35-6)

Guidance literature:

Multi-step reaction with 6 steps

1: 98 percent / pyridinium p-toluenesulfonate / CH₂Cl₂ / 4 h / Ambient temperature

2: 1) magnesium, 2) Li₂CuCl₄ / 1) THF, 2) room temperature, 3 h

3: NaOH / ethanol / 2 h / Heating

4: 2 N HCl / ethanol / 1 h / Heating

5: pyridine / CHCl₃ / 5 h / Ambient temperature

6: pyridine / 2 h / Ambient temperature

With pyridine; hydrogenchloride; sodium hydroxide; dilithium tetrachlorocuprate; pyridinium p-toluenesulfonate; magnesium; In ethanol; dichloromethane; chloroform;

upstream raw materials:

24-((9Z,12Z)-Octadeca-9,12-dienoyloxy)-tetracosanoic acid

1-nitro-4-trifluoroacetoxy-benzene

linoleyl chloride

1,13-tridecanediol

Refernces