1,2,3,5-Cyclohexanetetrol

Base Information

• Chemical Name: 1,2,3,5-Cyclohexanetetrol
• CAS No.: 136936-97-5
• Molecular Formula: C6H12O4
• Molecular Weight: 148.159
• Mol file: 136936-97-5.mol

Synonyms:

Chemical Property of 1,2,3,5-Cyclohexanetetrol

Chemical Property:

Purity/Quality:

99.90% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,2,3,5-Cyclohexanetetrol

There total 3 articles about 1,2,3,5-Cyclohexanetetrol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(+/-)-4c,6t-Dibrom-1r,2c,3c,5t-tetrahydroxy-cyclohexan (6090-94-4,89673-82-5) → cyclohexanetetrol-(1r,2c,3c,5t) (3877-36-9,53585-08-3,64396-74-3,136936-97-5)

Guidance literature:

With ion-exchange resin + form>; hydrogen; nickel; In water;

DOI:10.1021/jo01031a061

Reference yield:

O1,O2;O3,O4-diisopropyliden-5,6-anhydro-allo-inositol (744209-88-9) → cyclohexanetetrol-(1r,2c,3c,5t) (3877-36-9,53585-08-3,64396-74-3,136936-97-5)

Guidance literature:

Multi-step reaction with 2 steps

1: (i) HBr, AcOH, (ii) Ac₂O, (iii) HCl, EtOH

2: H₂, ion-exchange resin + form> / Raney-Ni / H₂O

With ion-exchange resin + form>; hydrogen; nickel; In water;

DOI:10.1021/jo01031a061

Reference yield:

→ 1,3,4,5-tetrahydroxycyclohexane (136936-97-5)

Guidance literature:

(2), HCl;

DOI:10.7164/antibiotics.32.81

upstream raw materials:

(+/-)-4c,6t-Dibrom-1r,2c,3c,5t-tetrahydroxy-cyclohexan

O¹,O²;O³,O⁴-diisopropyliden-5,6-anhydro-allo-inositol

Refernces

• 1、 Mercer,Gero,Barnett. "The preparation of 1 D 2,6-dideoxy-[1-3H]-streptamine". . p. 81 - 82. Retrieved 2007/10/14.