Technology Process of Cyclohexanone, 2-[5-oxo-2-(phenylsulfonyl)hexyl]-
There total 4 articles about Cyclohexanone, 2-[5-oxo-2-(phenylsulfonyl)hexyl]- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
oxygen; copper(l) chloride; palladium dichloride;
In
water; dimethyl sulfoxide;
for 0.25h;
Heating;
DOI:10.1021/jo00022a042
- Guidance literature:
-
Multi-step reaction with 4 steps
1: TsOH*H2O, 3 Angstroem molecular sieves / benzene / 3 h / Heating
2: 1.) n-BuLi, 2.) HMPA / 1.) hexane, THF, -78 deg C, 20 min, 2.a) -30 deg C, 40 min, b) 0 deg C, 2 h
3: aq. HCl / tetrahydrofuran / 40 °C
4: 85 percent / PdCl2, CuCl, O2 / H2O; dimethylsulfoxide / 0.25 h / Heating
With
hydrogenchloride; N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; 3 A molecular sieve; oxygen; toluene-4-sulfonic acid; copper(l) chloride; palladium dichloride;
In
tetrahydrofuran; water; dimethyl sulfoxide; benzene;
DOI:10.1021/jo00022a042
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) n-BuLi, 2.) HMPA / 1.) hexane, THF, -78 deg C, 20 min, 2.a) -30 deg C, 40 min, b) 0 deg C, 2 h
2: aq. HCl / tetrahydrofuran / 40 °C
3: 85 percent / PdCl2, CuCl, O2 / H2O; dimethylsulfoxide / 0.25 h / Heating
With
hydrogenchloride; N,N,N,N,N,N-hexamethylphosphoric triamide; n-butyllithium; oxygen; copper(l) chloride; palladium dichloride;
In
tetrahydrofuran; water; dimethyl sulfoxide;
DOI:10.1021/jo00022a042