3-chloropropyl-2-furfurylsulfide

Base Information

• Chemical Name: 3-chloropropyl-2-furfurylsulfide
• CAS No.: 114914-08-8
• Molecular Formula: C₈H₁₁ClOS
• Molecular Weight: 190.694
• Mol file: 114914-08-8.mol

Synonyms:3-chloropropyl-2-furfurylsulfide

Chemical Property of 3-chloropropyl-2-furfurylsulfide

Chemical Property:

• Vapor Pressure: 0.0198mmHg at 25°C
• Boiling Point: 260.5°Cat760mmHg
• Flash Point: 111.3°C
• PSA: 34.53000
• Density: 1.166g/cm³
• LogP: 2.99870

Purity/Quality:

99%min ^*data from raw suppliers

2-([(3-CHLOROPROPYL)SULFANYL]METHYL)FURAN 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-chloropropyl-2-furfurylsulfide

There total 2 articles about 3-chloropropyl-2-furfurylsulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

aluminium trichloride (7446-70-0) + 2-thiolomethyl-furan (98-02-2,175236-33-6) + 1.3-chlorobromopropane (109-70-6) → (3-chloro-propyl)-furfuryl sulfide (114914-08-8)

Guidance literature:

With sodium methylate; In methanol;

Reference yield:

3-chloropropyl p-toluenesulfonate (632-02-0) + 2-thiolomethyl-furan (98-02-2,175236-33-6) → (3-chloro-propyl)-furfuryl sulfide (114914-08-8)

Guidance literature:

With diethyl ether; ethylmagnesium bromide;

DOI:10.1021/ja01368a069

upstream raw materials:

3-chloropropyl p-toluenesulfonate

2-thiolomethyl-furan

aluminium trichloride

1.3-chlorobromopropane

Refernces

• 1、 -. "7α-(ξ-aminoalkyl)-estratrienes, process for their production, pharmaceutical preparations which contain these 7α-(ξ-aminoalkyl)-estratrienes as well as their use for the production of pharmaceutical agents". . . Retrieved 2008/06/13.