2-Bromo-6-chloro-4-nitroaniline

Base Information Edit

Chemical Name:2-Bromo-6-chloro-4-nitroaniline
CAS No.:99-29-6
Molecular Formula:C6H4BrClN2O2
Molecular Weight:251.467
Hs Code.:2921420090
European Community (EC) Number:202-745-9
NSC Number:88985
UNII:XP2L34WT49
DSSTox Substance ID:DTXSID2059192
Nikkaji Number:J38.264G
Wikidata:Q72453142
Mol file:99-29-6.mol

Synonyms:2-Bromo-6-chloro-4-nitroaniline;99-29-6;2-Chloro-4-nitro-6-bromoaniline;6-Bromo-2-chloro-4-nitroaniline;Benzenamine, 2-bromo-6-chloro-4-nitro-;C6H4BrClN2O2;Aniline, 2-bromo-6-chloro-4-nitro-;2-Bromo-4-nitro-6-chloroaniline;2-Chloro-6-bromo-4-nitroaniline;2-bromo-6-chloro-4-nitrobenzenamine;XP2L34WT49;EINECS 202-745-9;NSC 88985;NSC-88985;6-bromo-2-chloro-4-nitrophenylamine;NSC88985;NCIOpen2_005688;UNII-XP2L34WT49;2-brom-6-chlor-4-nitroanilin;SCHEMBL2069936;C6-H4-Br-Cl-N2-O2;DTXSID2059192;GLUCALKKMFBJEB-UHFFFAOYSA-;MFCD00014770;STL508688;AKOS005354318;AC-4383;2-Bromo-6-chloro-4-nitroaniline, 98%;AS-60491;AM20050214;B1771;FT-0611509;D88857;EN300-6732631;A845994;W-100044;N-[6-[[3-acetamido-4,5-dihydroxy-6-(hydroxymethyl)tetrahydropyran-2-yl]oxymethyl]-2-benzyl-5-hydroxy-4-(3,4,5-trihydroxy-6-methyl-tetrahydropyran-2-yl)oxy-tetrahydropyran-3-yl]acetamide

Suppliers and Price of 2-Bromo-6-chloro-4-nitroaniline

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TCI Chemical
2-Bromo-6-chloro-4-nitroaniline >98.0%(GC)
25g
$ 23.00

Sigma-Aldrich
2-Bromo-6-chloro-4-nitroaniline 98%
25g
$ 153.00

Matrix Scientific
2-Bromo-6-chloro-4-nitroaniline 95+%
100g
$ 101.00

Matrix Scientific
2-Bromo-6-chloro-4-nitroaniline 95+%
10g
$ 24.00

Crysdot
2-Bromo-6-chloro-4-nitroaniline 95+%
100g
$ 89.00

Biosynth Carbosynth
2-Chloro-4-nitro-6-bromoaniline
10 g
$ 50.00

Biosynth Carbosynth
2-Chloro-4-nitro-6-bromoaniline
250 g
$ 577.50

Biosynth Carbosynth
2-Chloro-4-nitro-6-bromoaniline
100 g
$ 289.00

Biosynth Carbosynth
2-Chloro-4-nitro-6-bromoaniline
50 g
$ 170.00

Biosynth Carbosynth
2-Chloro-4-nitro-6-bromoaniline
25 g
$ 100.00

Total 68 raw suppliers

Chemical Property of 2-Bromo-6-chloro-4-nitroaniline Edit

Chemical Property:

Appearance/Colour:Pale Yellow Powder
Vapor Pressure:6.47E-05mmHg at 25°C
Melting Point:176-178 °C(lit.)
Refractive Index:1.677
Boiling Point:344.7 °C at 760 mmHg
PKA:-3.31±0.20(Predicted)
Flash Point:162.3 °C
PSA：71.84000
Density:1.909 g/cm³
LogP:3.69730
Storage Temp.:Keep in dark place,Inert atmosphere,Room temperature
XLogP3:2.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:0
Exact Mass:249.91447
Heavy Atom Count:12
Complexity:187

Purity/Quality:: 2-Bromo-6-chloro-4-nitroaniline >98.0%(GC) ^*data from reagent suppliers

Safty Information:

Pictogram(s): Xi
Hazard Codes:Xi
Statements: 36/37/38
Safety Statements: 26-36

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=C(C=C(C(=C1Cl)N)Br)[N+](=O)[O-]

Technology Process of 2-Bromo-6-chloro-4-nitroaniline

There total 10 articles about 2-Bromo-6-chloro-4-nitroaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.62%

: 121-87-9
2-Chloro-4-nitroaniline

: 99-29-6
1-amino-2-bromo-4-nitro-6-chlorobenzene

Guidance literature:: With sodium chlorate; sulfuric acid; hydrogen bromide; In water; at 35 - 65 ℃;

Reference yield: 90.0%

: 13296-94-1
2-bromo-4-nitroaniline

: 99-29-6
1-amino-2-bromo-4-nitro-6-chlorobenzene

Guidance literature:: With sodium periodate; sulfuric acid; sodium dodecyl-sulfate; acetic acid; sodium chloride; In water; at 25 ℃; for 1h;
DOI:10.1080/00397911.2011.589560

Reference yield:

: 95-50-1
1,2-dichloro-benzene

: 99-29-6
1-amino-2-bromo-4-nitro-6-chlorobenzene

Guidance literature:: Multi-step reaction with 3 steps

1: sulfuric acid; sulfur trioxide; nitric acid / water / 30 - 60 °C

2: tetrabutylammomium bromide; copper(l) chloride; ammonium hydroxide / water / 140 °C / 24002.4 Torr

3: sulfuric acid; hydrogen bromide; sodium chlorate / water / 35 - 65 °C

With sodium chlorate; ammonium hydroxide; sulfuric acid; sulfur trioxide; tetrabutylammomium bromide; hydrogen bromide; nitric acid; copper(l) chloride; In water;