4,4'-Di(benzenesulfonyl)-1,1'-biphenyl

Base Information

• Chemical Name: 4,4'-Di(benzenesulfonyl)-1,1'-biphenyl
• CAS No.: 1433-00-7
• Molecular Formula: C24H18O4S2
• Molecular Weight: 434.537
• DSSTox Substance ID: DTXSID50562845
• Nikkaji Number: J2.973.183G
• Wikidata: Q82447132
• Mol file: 1433-00-7.mol

Synonyms:4,4'-Di(benzenesulfonyl)-1,1'-biphenyl;1433-00-7;SCHEMBL197508;DTXSID50562845

Chemical Property of 4,4'-Di(benzenesulfonyl)-1,1'-biphenyl

Chemical Property:

• XLogP3: 5.1
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 5
• Exact Mass: 434.06465140
• Heavy Atom Count: 30
• Complexity: 668

Purity/Quality:

99.90% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)S(=O)(=O)C2=CC=C(C=C2)C3=CC=C(C=C3)S(=O)(=O)C4=CC=CC=C4

Technology Process of 4,4'-Di(benzenesulfonyl)-1,1'-biphenyl

There total 6 articles about 4,4'-Di(benzenesulfonyl)-1,1'-biphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

biphenyl (92-52-4,1594-86-1) + benzenesulfonyl chloride (98-09-9) → 4,4'-bis-benzenesulfonyl-biphenyl (1433-00-7)

Guidance literature:

With iron(III) chloride; at 80 - 140 ℃;

Reference yield:

4,4'-di(phenylthio)-1,1'-biphenyl (2974-07-4) → 4,4'-bis-benzenesulfonyl-biphenyl (1433-00-7)

Guidance literature:

With dihydrogen peroxide; acetic acid;

Reference yield:

4,4'-dichlorobiphenyl (2050-68-2) → 4,4'-bis-benzenesulfonyl-biphenyl (1433-00-7)

Guidance literature:

Multi-step reaction with 2 steps

1: quinoline; pyridine

2: aqueous H₂O₂; acetic acid

With pyridine; quinoline; dihydrogen peroxide; acetic acid;

upstream raw materials:

4,4'-di(phenylthio)-1,1'-biphenyl

biphenyl

benzenesulfonyl chloride

trimethylphenylsilane