Germanamine, 1-chloro-1,1-diethyl-N-(2,4,6-trimethylphenyl)-

Base Information

• Chemical Name: Germanamine, 1-chloro-1,1-diethyl-N-(2,4,6-trimethylphenyl)-
• CAS No.: 143367-71-9
• Molecular Formula: C₁₃H₂₂ClGeN
• Molecular Weight: 300.367
• Mol file: 143367-71-9.mol

Synonyms:

Chemical Property of Germanamine, 1-chloro-1,1-diethyl-N-(2,4,6-trimethylphenyl)-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of Germanamine, 1-chloro-1,1-diethyl-N-(2,4,6-trimethylphenyl)-

There total 1 articles about Germanamine, 1-chloro-1,1-diethyl-N-(2,4,6-trimethylphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

diethyl germanium dichloride (13314-52-8) + 2,4,6-trimethylaniline (88-05-1) → N-diethylchlorogermyl-N-mesitylamine (143367-71-9)

Guidance literature:

With triethylamine; In benzene; byproducts: (C2H5)3NHCl; under inert gas; xaddn. of soln. of (C2H5)2GeCl2 (15 mmol) in benzene to mixt. of C6H2(CH3)3NH2 (15 mmol) and (C2H5)3N (50 mmol); stirring for 17 h at 20°C;; removing (C2H5)3NHCl and distg. filtrate (short column to avoid thermal decompn.); elem. anal.;;

upstream raw materials:

diethyl germanium dichloride

2,4,6-trimethylaniline