Technology Process of Carbamic acid,
[2-[(2-hydroxyethyl)amino]-2-oxo-1-[[4-(phenylmethoxy)phenyl]methyl]eth
yl]-, 1,1-dimethylethyl ester, (S)-
There total 1 articles about Carbamic acid,
[2-[(2-hydroxyethyl)amino]-2-oxo-1-[[4-(phenylmethoxy)phenyl]methyl]eth
yl]-, 1,1-dimethylethyl ester, (S)- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium tetrahydroborate; lithium chloride;
In
tetrahydrofuran; ethanol;
for 20h;
Ambient temperature;
- Guidance literature:
-
With
carbon tetrabromide; triphenylphosphine;
In
dichloromethane;
for 20h;
Ambient temperature;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 74 percent / CBr4, Ph3P / CH2Cl2 / 20 h / Ambient temperature
2: 90 percent / dimethylformamide / 20 h / Ambient temperature
3: HCOOH, 30percent H2O2 / 20 h / Ambient temperature
4: H2, 98percent aq. HCOOH, 30percent H2O2 / 10percent Pd/C / 10 h
With
formic acid; carbon tetrabromide; hydrogen; dihydrogen peroxide; triphenylphosphine;
palladium on activated charcoal;
In
dichloromethane; N,N-dimethyl-formamide;