Technology Process of 2-Propanol, 1-[(4-methoxyphenyl)methoxy]-3-(octadecyloxy)-, (R)-
There total 4 articles about 2-Propanol, 1-[(4-methoxyphenyl)methoxy]-3-(octadecyloxy)-, (R)- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
batyl alcohol;
With
di(n-butyl)tin oxide;
In
toluene;
for 2h;
Reflux;
Dean-Stark;
With
cesium fluoride;
for 1.5h;
p-methoxybenzyl chloride;
In
N,N-dimethyl-formamide;
regioselective reaction;
Inert atmosphere;
DOI:10.3390/molecules21010047
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: toluene-4-sulfonic acid / methanol / 8 h
2.1: di(n-butyl)tin oxide / toluene / 2 h / Reflux; Dean-Stark
2.2: 1.5 h
2.3: Inert atmosphere
With
di(n-butyl)tin oxide; toluene-4-sulfonic acid;
In
methanol; toluene;
DOI:10.3390/molecules21010047
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium amide / toluene / 1 h / 111 °C / Inert atmosphere
1.2: 3 h / 20 - 111 °C / Inert atmosphere
2.1: toluene-4-sulfonic acid / methanol / 8 h
3.1: di(n-butyl)tin oxide / toluene / 2 h / Reflux; Dean-Stark
3.2: 1.5 h
3.3: Inert atmosphere
With
di(n-butyl)tin oxide; toluene-4-sulfonic acid; sodium amide;
In
methanol; toluene;
1.1: |Williamson Ether Synthesis / 1.2: |Williamson Ether Synthesis;
DOI:10.3390/molecules21010047
