2-Propenoic acid, 3-phenyl-, 2-hydroxyethyl ester, (E)-

Base Information

• Chemical Name: 2-Propenoic acid, 3-phenyl-, 2-hydroxyethyl ester, (E)-
• CAS No.: 146604-63-9
• Molecular Formula: C11H12O3
• Molecular Weight: 192.214
• Mol file: 146604-63-9.mol

Synonyms:

Chemical Property of 2-Propenoic acid, 3-phenyl-, 2-hydroxyethyl ester, (E)-

Chemical Property:

Purity/Quality:

99.90% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-Propenoic acid, 3-phenyl-, 2-hydroxyethyl ester, (E)-

There total 15 articles about 2-Propenoic acid, 3-phenyl-, 2-hydroxyethyl ester, (E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

(E)-3-phenylacrylic acid (140-10-3) + ethylene glycol (107-21-1) → 2-hydroxyethyl 3-(phenyl)-2-propenoate (146604-63-9)

Guidance literature:

With sulfuric acid; In toluene; Heating;

DOI:10.1016/0031-9422(93)85004-B

Reference yield: 93.0%

C17H26O3Si → 2-hydroxyethyl 3-(phenyl)-2-propenoate (146604-63-9)

Guidance literature:

With Povidone-Iodine; In methanol; at 30 ℃; for 1h;

DOI:10.1016/j.tetlet.2019.05.059

Reference yield: 88.0%

(E)-3-phenylpropenal (14371-10-9) + ethylene glycol (107-21-1) → 2-hydroxyethyl 3-(phenyl)-2-propenoate (146604-63-9)

Guidance literature:

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; Amberlyst 15; for 6h; Heating / reflux;

upstream raw materials:

2-((E)-Styryl)-[1,3]dioxolane

ethylene glycol

3-phenyl-propenal

iodobenzene

Downstream raw materials:

C₁₈H₁₄N₂O₄S

Refernces

• 1、 Ke, Yanxiong,Lu, Guangying,Ren, Jiangmeng,Wang, Di,Zeng, Bu-Bing. "Catalytic removal of tert-butyldimethylsilyl (TBS) ether by PVP-I". . . Retrieved 2019/09/06.
• 2、 Lee, Li-Chen,Zhao, Yan. "Interfacially cross-linked reverse micelles as soluble support for palladium nanoparticle catalysts". experimental part. p. 863 - 871. Retrieved 2012/08/08.