1-Naphthalenecarbamic acid, 2-chloroethyl ester

Base Information

• Chemical Name: 1-Naphthalenecarbamic acid, 2-chloroethyl ester
• CAS No.: 25216-25-5
• Molecular Formula: C13H12 Cl N O2
• Molecular Weight: 249.697
• European Community (EC) Number: 667-341-0
• NSC Number: 106881
• DSSTox Substance ID: DTXSID70179873
• Wikidata: Q83050388
• Mol file: 25216-25-5.mol

Synonyms:25216-25-5;1-NAPHTHALENECARBAMIC ACID, 2-CHLOROETHYL ESTER;CB 14;2-chloroethyl naphthalen-1-ylcarbamate;NSC 106881;BRN 3310939;Carbamic acid, 1-naphthalenyl-, 2-chloroethyl ester;DTXSID70179873;NSC106881;AKOS024335274;NSC-106881;LS-94443;2-CHLOROETHYL N-(1-NAPHTHYL)CARBAMATE;2-CHLOROETHYL N-(NAPHTHALEN-1-YL)CARBAMATE

Chemical Property of 1-Naphthalenecarbamic acid, 2-chloroethyl ester

Chemical Property:

• Vapor Pressure: 2.44E-05mmHg at 25°C
• Boiling Point: 359.1°Cat760mmHg
• Flash Point: 171°C
• Density: 1.308g/cm³
• XLogP3: 2.6
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 4
• Exact Mass: 249.0556563
• Heavy Atom Count: 17
• Complexity: 260

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C1=CC=C2C(=C1)C=CC=C2NC(=O)OCCCl

Technology Process of 1-Naphthalenecarbamic acid, 2-chloroethyl ester

There total 2 articles about 1-Naphthalenecarbamic acid, 2-chloroethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-Naphthyl isocyanate (86-84-0) + 2-chloro-ethanol (107-07-3) → [1]naphthyl-carbamic acid-(2-chloro-ethyl ester) (25216-25-5)

Guidance literature:

DOI:10.1016/0584-8539(83)80121-4

Reference yield:

1-amino-naphthalene (134-32-7) + 2-Chloroethyl chloroformate (627-11-2) → [1]naphthyl-carbamic acid-(2-chloro-ethyl ester) (25216-25-5)

Guidance literature:

Reference yield:

[1]naphthyl-carbamic acid-(2-chloro-ethyl ester) (25216-25-5) → N-(2-hydroxyethyl)-1-naphthylamine (2933-59-7)

Guidance literature:

With potassium hydroxide;

upstream raw materials:

1-amino-naphthalene

2-Chloroethyl chloroformate

1-Naphthyl isocyanate

2-chloro-ethanol

Downstream raw materials:

3-(α-naphthyl)-2-oxazolidinone

N-(2-hydroxyethyl)-1-naphthylamine

Refernces