(2,3-Dihydroxypropyl)trimethylammonium chloride

Base Information

• Chemical Name: (2,3-Dihydroxypropyl)trimethylammonium chloride
• CAS No.: 34004-36-9
• Deprecated CAS: 1883418-77-6
• Molecular Formula: C6H16 N O2 . Cl
• Molecular Weight: 169.652
• Hs Code.: 2923900090
• European Community (EC) Number: 251-783-2
• UNII: V5RP514IX5
• DSSTox Substance ID: DTXSID4052766
• Wikidata: Q27291567
• Mol file: 34004-36-9.mol

Synonyms:(2,3-dihydroxypropyl)trimethylammonium chloride;2,3-DHP-TACl

Chemical Property of (2,3-Dihydroxypropyl)trimethylammonium chloride

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• PSA: 40.46000
• Density: g/cm³
• LogP: -3.95020
• Storage Temp.: Inert atmosphere,Room Temperature
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 3
• Exact Mass: 169.0869564
• Heavy Atom Count: 10
• Complexity: 77.6

Purity/Quality:

98%Min ^*data from raw suppliers

2,3-Dihydroxy-N,N,N-trimethylpropan-1-aminiumchloride 95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C[N+](C)(C)CC(CO)O.[Cl-]

Technology Process of (2,3-Dihydroxypropyl)trimethylammonium chloride

There total 4 articles about (2,3-Dihydroxypropyl)trimethylammonium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

N-(3-chloro-2-hydroxypropyl)trimethylammonium chloride (101396-91-2,117604-42-9) → N-[(2,3-dihydroxy)prop-1-yl]-N,N,N-trimethylammonium chloride (34004-36-9)

Guidance literature:

With sodium hydroxide; In water; at 20 - 50 ℃; for 14h;

Reference yield: 91.2%

3-monochloro-1,2-propanediol (96-24-2) + trimethylamine (75-50-3) → N-[(2,3-dihydroxy)prop-1-yl]-N,N,N-trimethylammonium chloride (34004-36-9)

Guidance literature:

In water; at 90 ℃; for 16h;

Reference yield: 71.0%

oxiranyl-methanol (556-52-5) + trimethylamine hydrochloride (593-81-7) → N-[(2,3-dihydroxy)prop-1-yl]-N,N,N-trimethylammonium chloride (34004-36-9)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In methanol; at 20 ℃; for 12h;

DOI:10.1021/bc900469z

upstream raw materials:

3-monochloro-1,2-propanediol

trimethylamine

N-(3-chloro-2-hydroxypropyl)trimethylammonium chloride

oxiranyl-methanol

Downstream raw materials:

trimethylamine

(2,3-bis(3,3,4,4,5,5,6,6,7,7,8,8-dodecafluorotetradecanoyloxy)prop-1-yl)-N,N,N-trimethylammonium chloride

(2,3-bis(3,3,4,4,5,5,6,6-octafluorohexadecanoyloxy)prop-1yl)-N,N,N-trimethylammonium chloride

(2,3-bis(3,3,4,4,5,5,6,6,7,7,8,8-dodecafluorooctadecanoyloxy)prop-1-yl)-N,N,N-trimethylammonium chloride

Refernces

• 1、 Erfurt, Karol,Wandzik, Ilona,Walczak, Krzysztof,Matuszek, Karolina,Chrobok, Anna. "Hydrogen-bond-rich ionic liquids as effective organocatalysts for Diels-Alder reactions". . p. 3508 - 3514. Retrieved 2014/07/08.
• 2、 -. "PROCESS FOR PREPARING DIHYDROXYTRIALKYLAMMONIUM HALIDES AND PRODUCTS THEREOF". Page/Page column 12; 13. . Retrieved 2008/06/13.