Technology Process of Acetic acid, diazo-, cis-4-(1,1-dimethylethyl)cyclohexyl ester
There total 3 articles about Acetic acid, diazo-, cis-4-(1,1-dimethylethyl)cyclohexyl ester which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium hydroxide;
In
acetonitrile;
for 14h;
Ambient temperature;
DOI:10.1002/hlca.19940770307
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 72 percent / xylene / 0.5 h / Heating
2: 76 percent / methane sulfonyl azide, Et3N / acetonitrile / 3 h / Ambient temperature
3: 63 percent / 8 percent KOH / acetonitrile / 14 h / Ambient temperature
With
potassium hydroxide; triethylamine; Methanesulfonyl azide;
In
acetonitrile; xylene;
DOI:10.1002/hlca.19940770307
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 76 percent / methane sulfonyl azide, Et3N / acetonitrile / 3 h / Ambient temperature
2: 63 percent / 8 percent KOH / acetonitrile / 14 h / Ambient temperature
With
potassium hydroxide; triethylamine; Methanesulfonyl azide;
In
acetonitrile;
DOI:10.1002/hlca.19940770307
