9H-Carbazole-3-carboxylic acid, 2-hydroxy-

Base Information

• Chemical Name: 9H-Carbazole-3-carboxylic acid, 2-hydroxy-
• CAS No.: 14501-64-5
• Molecular Formula: C13H9NO3
• Molecular Weight: 227.219
• Hs Code.: 2933990090
• European Community (EC) Number: 238-508-1
• DSSTox Substance ID: DTXSID0065777
• Nikkaji Number: J241.271C
• Wikidata: Q72483460
• Mol file: 14501-64-5.mol

Synonyms:14501-64-5;2-hydroxy-9h-carbazole-3-carboxylic acid;9H-Carbazole-3-carboxylic acid, 2-hydroxy-;2-Hydroxycarbazole-3-carboxylic acid;EINECS 238-508-1;SCHEMBL1954200;2-hydroxycarbazole-3-carboxylic;DTXSID0065777;2-hydroxy-9h-carbazole-3-carboxylicacid;Carbazole-3-carboxylic acid, 2-hydroxy-;2-HYDROXYCARBAZOLE-3-CARBOXYLICACID

Chemical Property of 9H-Carbazole-3-carboxylic acid, 2-hydroxy-

Chemical Property:

• Vapor Pressure: 4.22E-12mmHg at 25°C
• Melting Point: 273-274 °C
• Refractive Index: 1.841
• Boiling Point: 530.9°C at 760mmHg
• PKA: 3.24±0.30(Predicted)
• Flash Point: 274.9°C
• PSA: 73.32000
• Density: 1.546g/cm³
• LogP: 2.72490
• XLogP3: 3.1
• Hydrogen Bond Donor Count: 3
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 1
• Exact Mass: 227.058243149
• Heavy Atom Count: 17
• Complexity: 320

Purity/Quality:

98%Min ^*data from raw suppliers

2-HYDROXYCARBANOLE-3-CARBOXYLIC ACID 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C2C(=C1)C3=CC(=C(C=C3N2)O)C(=O)O

Technology Process of 9H-Carbazole-3-carboxylic acid, 2-hydroxy-

There total 4 articles about 9H-Carbazole-3-carboxylic acid, 2-hydroxy- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 2-Hydroxycarbazole-3-carboxylic acid (14501-64-5) + 2-hydroxy-9H-carbazole-1-carboxylic acid (23077-32-9)

Guidance literature:

With carbon dioxide; 1,2-dichloro-benzene; at 150 ℃; under 2942.03 Torr;

Reference yield:

2-hydroxycarbazole (86-79-3) → 2-Hydroxycarbazole-3-carboxylic acid (14501-64-5) + 2-hydroxy-9H-carbazole-1-carboxylic acid (23077-32-9)

Guidance literature:

With carbon dioxide; potassium hydrogencarbonate; at 275 ℃; under 18387.7 Torr;

Reference yield:

mukonal (20323-67-5) → 2-Hydroxycarbazole-3-carboxylic acid (14501-64-5)

Guidance literature:

With manganese(IV) oxide; In tetrachloromethane; for 5h;

DOI:10.1016/S0031-9422(00)80360-X

upstream raw materials:

2-hydroxycarbazole

mukonal

Downstream raw materials:

girinimbine

3,3-Dimethyl-1-(toluene-4-sulfonyloxy)-1,2,3,11-tetrahydro-4-oxa-11-aza-benzo[a]fluorene-5-carboxylic acid methyl ester

Toluene-4-sulfonic acid 8,8-dimethyl-6,7,8,11-tetrahydro-9-oxa-11-aza-benzo[b]fluoren-6-yl ester

Refernces