Technology Process of Carbamic acid, [1-iodo-4-(phenylmethoxy)-2-naphthalenyl]-,
1,1-dimethylethyl ester
There total 10 articles about Carbamic acid, [1-iodo-4-(phenylmethoxy)-2-naphthalenyl]-,
1,1-dimethylethyl ester which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
iodine; iodic acid;
In
methanol; water;
at 80 ℃;
for 5h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: benzhydrylidene(methyl)amine; 20% palladium hydroxide-activated charcoal / toluene / 6 h / 100 °C / Sealed tube; Inert atmosphere
1.2: 48 h / 3102.97 Torr
2.1: potassium carbonate; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 3 h / 20 °C / Inert atmosphere
3.1: toluene-4-sulfonic acid / tetrahydrofuran / 0.17 h / -20 °C / Inert atmosphere
3.2: 4 h / -20 - 20 °C
With
20% palladium hydroxide-activated charcoal; benzhydrylidene(methyl)amine; tetra-(n-butyl)ammonium iodide; potassium carbonate; toluene-4-sulfonic acid;
In
tetrahydrofuran; N,N-dimethyl-formamide; toluene;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: potassium carbonate; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 3 h / 20 °C / Inert atmosphere
2.1: toluene-4-sulfonic acid / tetrahydrofuran / 0.17 h / -20 °C / Inert atmosphere
2.2: 4 h / -20 - 20 °C
With
tetra-(n-butyl)ammonium iodide; potassium carbonate; toluene-4-sulfonic acid;
In
tetrahydrofuran; N,N-dimethyl-formamide;