3,5-Dibromobiphenyl-2-amine

Base Information

• Chemical Name: 3,5-Dibromobiphenyl-2-amine
• CAS No.: 16372-95-5
• Molecular Formula: C12H9Br2N
• Molecular Weight: 327.01500
• Hs Code.: 2921499090
• Mol file: 16372-95-5.mol

Synonyms:3,5-Dibromo-biphenyl-2-ylamine;3,5-Dibromobiphenyl-2-amine;2,4-Dibromo-6-phenylamiline;

Chemical Property of 3,5-Dibromobiphenyl-2-amine

Chemical Property:

• PSA: 26.02000
• LogP: 5.04200

Purity/Quality:

99% ^*data from raw suppliers

3,5-Dibromo-[1,1'-biphenyl]-2-amine 95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3,5-Dibromobiphenyl-2-amine

There total 14 articles about 3,5-Dibromobiphenyl-2-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-phenylaniline (90-41-5) → 2.4-Dibrom-6-phenylanilin (16372-95-5)

Guidance literature:

With bromine; sodium acetate; acetic acid;

Reference yield:

2-azido-5-bromo-1,1'-biphenyl (91330-91-5) → 2.4-Dibrom-6-phenylanilin (16372-95-5)

Guidance literature:

With hydrogen bromide; acetic acid;

DOI:10.1021/ja01150a008

Reference yield:

2-azidobiphenyl (7599-23-7) → 2.4-Dibrom-6-phenylanilin (16372-95-5)

Guidance literature:

Multi-step reaction with 3 steps

1: acetic acid; HBr

2: aqueous NaN₃ / Diazotization

3: acetic acid; HBr

With sodium azide; hydrogen bromide; acetic acid;

DOI:10.1021/ja01150a008

upstream raw materials:

2-azido-5-bromo-1,1'-biphenyl

N-(5-bromo-[1,1'-biphenyl]-2-yl)acetamide

2-phenylaniline

bromine

Downstream raw materials:

N-(3,5-dibromo-biphenyl-2-yl)-benzamide

3.5-Dibrom-2-azidobiphenyl

3,5-dibromo-1,1′-biphenyl

Refernces