gamma-propanol

Base Information

• Chemical Name: gamma-propanol
• CAS No.: 36294-23-2
• Molecular Formula: C17H28 O2
• Molecular Weight: 264.408
• Hs Code.: 2907299090
• Mol file: 36294-23-2.mol

Synonyms:1-Propanol,3-(3,5-di-tert-butyl-4-hydroxyphenyl)- (7CI);2,6-Di-tert-butyl-4-(3-hydroxypropyl)phenol; 3,5-Bis(1,1-dimethylethyl)-4-hydroxybenzenepropanol;3,5-Di-tert-butyl-4-hydroxybenzenepropanol;3-(3,5-Di-tert-butyl-4-hydroxyphenyl)-1-propanol;3-(3,5-Di-tert-butyl-4-hydroxyphenyl)propanol;3-(3,5-Di-tert-butyl-4-hydroxyphenyl)propyl alcohol; 4-(3-Hydroxypropyl)-2,6-di-tert-butylphenol

Chemical Property of gamma-propanol

Chemical Property:

• Vapor Pressure: 2.94E-05mmHg at 25°C
• Boiling Point: 342.2°Cat760mmHg
• Flash Point: 146.1°C
• PSA: 40.46000
• Density: 0.986g/cm³
• LogP: 3.91210

Purity/Quality:

99%min ^*data from raw suppliers

2,6-DI-TERT-BUTYL-4-(3-HYDROXY-PROPYL)-PHENOL 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of gamma-propanol

There total 9 articles about gamma-propanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

4-hydroxy-3,5-di-tert-butylphenylpropionic acid (20170-32-5,90804-34-5) → 4-(3-hydroxypropyl)-2,6-di-tert-butylphenol (36294-23-2)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; Heating;

DOI:10.1021/jm990945v

Reference yield: 69.0%

2,6-di-tert-butylphenol (128-39-2) + allyl alcohol (107-18-6) → 4-(3-hydroxypropyl)-2,6-di-tert-butylphenol (36294-23-2) + 3-(3,5-di-tert-butyl-4-hydroxyphenyl)propyl 3-(3,5-di-tert-butyl-4-hydroxyphenyl)propionate (75546-73-5)

Guidance literature:

2,6-di-tert-butylphenol; With sodium hydroxide; at 130 ℃; for 2h; Autoclave; Inert atmosphere;

allyl alcohol; at 160 - 180 ℃; for 2.5h; Further stages; Autoclave; Inert atmosphere;

DOI:10.1134/S1070363210110101

Reference yield: 35.5%

→ 4-(3-hydroxypropyl)-2,6-di-tert-butylphenol (36294-23-2)

Guidance literature:

upstream raw materials:

4-hydroxy-3,5-di-tert-butylphenylpropionic acid

3,5-di-tert-butyl-4-hydroxycinnamic acid

methyl 3-(4-hydroxy-3,5-di-tert-butyl)phenylpropanoate

2,6-di-tert-butylphenol

Downstream raw materials:

7,9-di-tert-butyl-1-oxaspiro<4.5>deca-6,9-dien-8-one

2,6-Di-tert-butyl-4-(3-hydroxy-propyl)-4-methoxy-cyclohexa-2,5-dienone

2-<3-(4-hydroxy-3,5-di-tert-butylphenyl)propoxy>-4-pentyl-6-trichloromethyl-sym-triazine

C₄₂H₆₅N₃O₄

Refernces

• 1、 -. "Synthesis of benzotriazole monomer". Page/Page column 15. . Retrieved 2010/12/26.
• 2、 Oleynik,Kuprina,Pevneva,Markov,Kandalintseva,Prosenko,Grigor'ev. "Synthesis and antioxidant properties of sodium S-[3-(hydroxyaryl)propyl] thiosulfates and [3-(hydroxyaryl)propane]-1-sulfonates". . p. 1135 - 1143. Retrieved 2008/09/17.