4-Ethoxy-3-methoxybenzaldehydeethyleneacetal

Base Information Edit

Chemical Name:4-Ethoxy-3-methoxybenzaldehydeethyleneacetal
CAS No.:52987-93-6
Molecular Formula:C12H16O4
Molecular Weight:224.257
Hs Code.:2932999099
Mol file:52987-93-6.mol

Synonyms:3-Methoxy-4-ethoxybenzaldehydethylenacetal;

Suppliers and Price of 4-Ethoxy-3-methoxybenzaldehydeethyleneacetal

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
2-(4-ETHOXY-3-METHOXYPHENYL)-1,3-DIOXOLANE 95.00%
5G
$ 909.56

Total 3 raw suppliers

Chemical Property of 4-Ethoxy-3-methoxybenzaldehydeethyleneacetal Edit

Chemical Property:

Vapor Pressure:0.000602mmHg at 25°C
Boiling Point:320.2°Cat760mmHg
Flash Point:124.2°C
PSA：36.92000
Density:1.124g/cm³
LogP:2.13930

Purity/Quality:

99%min ^*data from raw suppliers

2-(4-ETHOXY-3-METHOXYPHENYL)-1,3-DIOXOLANE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4-Ethoxy-3-methoxybenzaldehydeethyleneacetal

There total 3 articles about 4-Ethoxy-3-methoxybenzaldehydeethyleneacetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 120-25-2
4-ethoxy-3-methoxybenzaldehyde

: 107-21-1
ethylene glycol

: 52987-93-6
2-(4-ethoxy-3-methoxyphenyl)-1,3-dioxolane

Guidance literature:: 4-ethoxy-3-methoxybenzaldehyde; ethylene glycol; With orthoformic acid triethyl ester; boron trifluoride diethyl etherate; In diethyl ether; at 100 ℃; for 24h; Heating / reflux;

With sodium hydroxide; water; In diethyl ether; at 20 ℃;

Reference yield:

: 121-33-5,8014-42-4
vanillin

: 52987-93-6
2-(4-ethoxy-3-methoxyphenyl)-1,3-dioxolane

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 0.17 h / 40 °C

1.2: 70 °C

2.1: toluene-4-sulfonic acid / benzene / 12 h / Reflux

With potassium carbonate; toluene-4-sulfonic acid; In N,N-dimethyl-formamide; benzene;
DOI:10.1016/j.cclet.2015.05.003