Triethylamine sulfamate

Base Information

• Chemical Name: Triethylamine sulfamate
• CAS No.: 761-02-4
• Molecular Formula: C6H18N2O3S
• Molecular Weight: 198.287
• European Community (EC) Number: 212-087-4
• DSSTox Substance ID: DTXSID0061082
• Mol file: 761-02-4.mol

Synonyms:Triethylamine sulfamate;Triethylammonium sulphamate;761-02-4;EINECS 212-087-4;C6H15N.H3NO3S;SCHEMBL2397671;DTXSID0061082;amidosulfuric acid triethylamine salt;C6-H15-N.H3-N-O3-S

Chemical Property of Triethylamine sulfamate

Chemical Property:

• Vapor Pressure: 56.1mmHg at 25°C
• Boiling Point: 90.5°C at 760 mmHg
• Flash Point: 152.2°C
• PSA: 92.01000
• LogP: 1.87710
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 3
• Exact Mass: 198.10381361
• Heavy Atom Count: 12
• Complexity: 118

Purity/Quality:

99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: CCN(CC)CC.NS(=O)(=O)O

Technology Process of Triethylamine sulfamate

There total 2 articles about Triethylamine sulfamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

triethylamine (121-44-8) → Triethylammoniumsalz der Amidosulfonsaeure (761-02-4)

Guidance literature:

With aminosulfonic acid; Inert atmosphere;

DOI:10.1016/j.molliq.2018.06.059

Reference yield:

4-methyleneoxetan-2-one (674-82-8,2130-41-8) + triethylamine (121-44-8) → Triethylammoniumsalz der Amidosulfonsaeure (761-02-4)

Guidance literature:

triethylamine; With aminosulfonic acid; acetic acid; In dichloromethane;

4-methyleneoxetan-2-one; In dichloromethane; Reagent/catalyst; Further stages;

Reference yield:

Triethylammoniumsalz der Amidosulfonsaeure (761-02-4) → potassium acesulfame (55589-62-3)

Guidance literature:

Triethylammoniumsalz der Amidosulfonsaeure; With sulfur trioxide; In dichloromethane;

With water;

With potassium hydroxide;

upstream raw materials:

triethylamine

4-methyleneoxetan-2-one

Downstream raw materials:

potassium acesulfame

Refernces

• 1、 Shmukler,Gruzdev,Kudryakova,Fadeeva, Yu A.,Kolker,Safonova. "Triethylammonium-based protic ionic liquids with sulfonic acids: Phase behavior and electrochemistry". . p. 139 - 146. Retrieved 2018/06/26.