Chlorodimethyl(octyloxy)silane

Base Information

• Chemical Name: Chlorodimethyl(octyloxy)silane
• CAS No.: 52322-14-2
• Molecular Formula: C10H23ClOSi
• Molecular Weight: 222.831
• DSSTox Substance ID: DTXSID00200346
• Wikidata: Q83073435
• Mol file: 52322-14-2.mol

Synonyms:Chlorodimethyl(octyloxy)silane;chloro-dimethyl-octoxysilane;52322-14-2;Dimethyloctoxychlorosilane;Silane, chlorodimethyl(octyloxy)-;BRN 5327462;C10H23ClOSi;chlorodimethyloctyloxysilane;C10-H23-Cl-O-Si;SCHEMBL3446738;DTXSID00200346;AKOS016013810;LS-145146

Chemical Property of Chlorodimethyl(octyloxy)silane

Chemical Property:

• Vapor Pressure: 0.0942mmHg at 25°C
• Boiling Point: 231.5°Cat760mmHg
• Flash Point: 79.1°C
• PSA: 9.23000
• Density: 0.901g/cm³
• LogP: 4.30410
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 8
• Exact Mass: 222.1206696
• Heavy Atom Count: 13
• Complexity: 118

Purity/Quality:

98%Min ^*data from raw suppliers

CHLORODIMETHYL(OCTYLOXY)SILANE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCCCCCCCO[Si](C)(C)Cl

Technology Process of Chlorodimethyl(octyloxy)silane

There total 1 articles about Chlorodimethyl(octyloxy)silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

octanol (111-87-5) + C12H24Cl2O6Si2 → diethyl (2R,3R)-tartrate (87-91-2) + dimethyl-bis-octyloxy-silane (18536-88-4) + chloro(dimethyl)octyloxysilane (52322-14-2)

Guidance literature:

With gallium(III) trichloride; at 20 ℃; for 6h; Inert atmosphere;

DOI:10.1039/b804589e

Reference yield: 87.0%

chloro(dimethyl)octyloxysilane (52322-14-2) + phenyl 2,3-O-isopropylidene-1-thio-α-D-ribofuranoside (153984-49-7) → ((3aR,4R,6R,6aR)-2,2-Dimethyl-6-phenylsulfanyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethoxy)-dimethyl-octyloxy-silane (157428-33-6)

Guidance literature:

With pyridine; In tetrahydrofuran;

DOI:10.1246/cl.1994.1049

Reference yield: 77.0%

chloro(dimethyl)octyloxysilane (52322-14-2) + methyl 2,4,6-tri-O-benzyl-1-thio-β-D-glucopyranoside (140420-80-0) → ((2R,3R,4S,5R,6S)-3,5-Bis-benzyloxy-2-benzyloxymethyl-6-methylsulfanyl-tetrahydro-pyran-4-yloxy)-dimethyl-octyloxy-silane

Guidance literature:

With pyridine; In tetrahydrofuran;

DOI:10.1246/cl.1994.1049

upstream raw materials:

octanol

Downstream raw materials:

phenyl 3,4,6-tri-O-acetyl-2-O--α-D-gluco-1-thiopyranoside

((3aR,4R,6R,6aR)-2,2-Dimethyl-6-phenylsulfanyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethoxy)-dimethyl-octyloxy-silane

octyl 2,3,4-tri-O-benzyl-β-D-glucopyranoside

octyl 2,4,6-tri-O-benzyl-β-D-glucopyranoside

Refernces