ALLYLSULFANYL-ACETIC ACID

Base Information

• Chemical Name: ALLYLSULFANYL-ACETIC ACID
• CAS No.: 20600-63-9
• Molecular Formula: C5H8O2S
• Molecular Weight: 132.1808
• Hs Code.: 2930909090
• Mol file: 20600-63-9.mol

Synonyms:allylsulfanyl-acetic acid;allylmercapto-acetic acid;allylthioacetic acid;Allylmercapto-essigsaeure;

Chemical Property of ALLYLSULFANYL-ACETIC ACID

Chemical Property:

• Vapor Pressure: 0.0109mmHg at 25°C
• Boiling Point: 242.9°Cat760mmHg
• PKA: 3.74±0.10(Predicted)
• Flash Point: 100.7°C
• PSA: 62.60000
• Density: 1.151g/cm³
• LogP: 0.99020

Purity/Quality:

98%min ^*data from raw suppliers

2-(Prop-2-en-1-ylsulfanyl)aceticAcid ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of ALLYLSULFANYL-ACETIC ACID

There total 3 articles about ALLYLSULFANYL-ACETIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

prop-2-ene-1-thiol (870-23-5) + sodium monochloroacetic acid (3926-62-3) → allylsulfanyl-acetic acid (20600-63-9)

Guidance literature:

prop-2-ene-1-thiol; With sodium ethanolate; In ethanol; at 0 - 20 ℃; for 1h;

sodium monochloroacetic acid; In ethanol; for 18h; Reflux;

With hydrogenchloride; water; In THFytetrahydrofuranethanol;

DOI:10.1021/jo801668b

Reference yield:

mercaptoacetic acid (68-11-1) + allyl bromide (106-95-6) → allylsulfanyl-acetic acid (20600-63-9)

Guidance literature:

With sodium hydroxide;

DOI:10.1021/ja01189a003

Reference yield:

→ allylsulfanyl-acetic acid (20600-63-9)

Guidance literature:

upstream raw materials:

mercaptoacetic acid

allyl bromide

prop-2-ene-1-thiol

sodium monochloroacetic acid

Downstream raw materials:

Allylthioglykolsaeurechlorid

Allylmercaptomethyl-penicillin

4,6-O-benzylidene-3-O-(allylthioacetyl)-D-allal

Refernces