Technology Process of Ferrocene, 1,1'-diacetyl-
There total 11 articles about Ferrocene, 1,1'-diacetyl- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
aluminium chloride;
In
dichloromethane;
ferrocene (1.0 equiv.) added to a stirred suspension of acetyl chloride (2.2 equiv.) and aluminium chloride (2.2 equiv.) in dichloromethane, stirred at room temp. overnight (16 h); washed with water, organic layer passed through a plug of alumina, washed with chloroform, washings concentrated in vacuo, crude product purified by flash column chromy. on silica gel (TLC Rf 0.24 (1:3 acetone-hexane)), elem. anal.;
DOI:10.1039/b000833h