Technology Process of Acetic acid, diazo-, 3-[3-methoxy-4-(phenylmethoxy)phenyl]propyl ester
There total 4 articles about Acetic acid, diazo-, 3-[3-methoxy-4-(phenylmethoxy)phenyl]propyl ester which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 100 percent / SOCl2 / Ambient temperature
2: 92 percent / K2CO3, 18-crown-6 / toluene / Heating
3: 95 percent / LiAlH4 / tetrahydrofuran / 3 h / Heating
4: 1.) Et3N, 2.) Et3N, MsN3, 3.) LiOH*H2O
With
lithium hydroxide; lithium aluminium tetrahydride; thionyl chloride; 18-crown-6 ether; potassium carbonate; triethylamine; Methanesulfonyl azide;
In
tetrahydrofuran; toluene;
DOI:10.1021/jo961607u
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 92 percent / K2CO3, 18-crown-6 / toluene / Heating
2: 95 percent / LiAlH4 / tetrahydrofuran / 3 h / Heating
3: 1.) Et3N, 2.) Et3N, MsN3, 3.) LiOH*H2O
With
lithium hydroxide; lithium aluminium tetrahydride; 18-crown-6 ether; potassium carbonate; triethylamine; Methanesulfonyl azide;
In
tetrahydrofuran; toluene;
DOI:10.1021/jo961607u
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 95 percent / LiAlH4 / tetrahydrofuran / 3 h / Heating
2: 1.) Et3N, 2.) Et3N, MsN3, 3.) LiOH*H2O
With
lithium hydroxide; lithium aluminium tetrahydride; triethylamine; Methanesulfonyl azide;
In
tetrahydrofuran;
DOI:10.1021/jo961607u