5-bromo-1-nitro-naphthalene

Base Information

• Chemical Name: 5-bromo-1-nitro-naphthalene
• CAS No.: 5328-76-7
• Molecular Formula: C10H6BrNO2
• Molecular Weight: 252.067
• Hs Code.: 2904909090
• Mol file: 5328-76-7.mol

Synonyms:1-Bromo-5-nitronaphthalene;5-Bromo-1-nitronaphthalene;5-bromo-1-nitro-naphthalene;1/C10H6BrNO2/c11-9-5-1-4-8-7(9)3-2-6-10(8)12(13)14/h1-6;10023-28-6;

Chemical Property of 5-bromo-1-nitro-naphthalene

Chemical Property:

• Vapor Pressure: 3.68E-05mmHg at 25°C
• Melting Point: 121 °C
• Refractive Index: 1.696
• Boiling Point: 363.8 °C at 760 mmHg
• Flash Point: 173.8 °C
• PSA: 45.82000
• Density: 1.662g/cm³
• LogP: 4.03370
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

99% ^*data from raw suppliers

1-Bromo-5-nitronaphthalene ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Technology Process of 5-bromo-1-nitro-naphthalene

There total 5 articles about 5-bromo-1-nitro-naphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

1-Nitronaphthalene (86-57-7) → 1-bromo-5-nitronaphthalene (5328-76-7)

Guidance literature:

With bromine; iron(III) chloride; at 90 ℃; for 2h;

DOI:10.1039/b413376e

Reference yield:

5-nitro-[1]naphthylamine (3272-91-1) → 1-bromo-5-nitronaphthalene (5328-76-7)

Guidance literature:

With sulfuric acid; acetic acid; Diazotization_.Behandlung der Diazoniumsalz-Loesung mit CuBr in konz. wss. HBr;

DOI:10.1039/jr9330001620

Reference yield:

1-Nitronaphthalene (86-57-7) + bromine (7726-95-6) → 1-bromo-5-nitronaphthalene (5328-76-7)

Guidance literature:

upstream raw materials:

1-Nitronaphthalene

5-nitro-[1]naphthylamine

bromine

iron(III) chloride

Downstream raw materials:

1-bromo-4,5-dinitronaphthalene

3-bromophthalic acid

5-amino-1-bromonaphthalene

(2-bromo-6-carboxy-phenyl)-glyoxylic acid

Refernces

• 1、 Antoniak, Damian,Barbasiewicz, Micha?. "Corey-Chaykovsky Cyclopropanation of Nitronaphthalenes: Access to Benzonorcaradienes and Related Systems". supporting information. p. 9320 - 9325. Retrieved 2019/11/19.
• 2、 -. "An electroluminescent compound and an electroluminescent device comprising the same". Paragraph 0390-0396. . Retrieved 2020/12/25.