2,2'-(1,2-Ethanediylbis(iminocarbonyl))bisbenzoic acid

Base Information

• Chemical Name: 2,2'-(1,2-Ethanediylbis(iminocarbonyl))bisbenzoic acid
• CAS No.: 62554-97-6
• Molecular Formula: C18H16 N2 O6
• Molecular Weight: 356.335
• European Community (EC) Number: 263-593-7
• UNII: B7H8N44X76
• DSSTox Substance ID: DTXSID20211595
• Nikkaji Number: J307.068I
• Wikidata: Q83086557
• Mol file: 62554-97-6.mol

Synonyms:62554-97-6;2,2'-(1,2-Ethanediylbis(iminocarbonyl))bisbenzoic acid;B7H8N44X76;EINECS 263-593-7;UNII-B7H8N44X76;2,2'-(ethane-1,2-diyldicarbamoyl)dibenzoic acid;2,2'-[1,2-ETHANEDIYLBIS(IMINOCARBONYL)]BISBENZOIC ACID;SCHEMBL10889755;DTXSID20211595;STK277337;AKOS005425726;2,2'-Ethylenebis(iminocarbonyl)dibenzoic acid;2,2'-(1,2-ETHANEDIYLBIS(IMINOCARBONYL))BIS(BENZOIC ACID);2-(2-((2-CARBOXYBENZOYL)AMINO)ETHYLCARBAMOYL)BENZOIC ACID;BENZOIC ACID, 2,2'-(1,2-ETHANEDIYLBIS(IMINOCARBONYL))BIS-

Chemical Property of 2,2'-(1,2-Ethanediylbis(iminocarbonyl))bisbenzoic acid

Chemical Property:

• Boiling Point: 722.5oC at 760 mmHg
• Flash Point: 390.8oC
• PSA: 139.78000
• Density: 1.391g/cm3
• LogP: 2.39240
• XLogP3: 1.2
• Hydrogen Bond Donor Count: 4
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 7
• Exact Mass: 356.10083623
• Heavy Atom Count: 26
• Complexity: 502

Purity/Quality:

98%Min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C(=C1)C(=O)NCCNC(=O)C2=CC=CC=C2C(=O)O)C(=O)O

Technology Process of 2,2'-(1,2-Ethanediylbis(iminocarbonyl))bisbenzoic acid

There total 3 articles about 2,2'-(1,2-Ethanediylbis(iminocarbonyl))bisbenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

phthalic anhydride (85-44-9) + ethylenediamine (107-15-3,85404-18-8) → N,N'-bis(2-carboxy-1-oxo-phenelenyl)ethylenediamine (62554-97-6)

Guidance literature:

In tetrahydrofuran; Heating;

DOI:10.1016/S1386-1425(02)00018-5

Reference yield:

→ N,N'-bis(2-carboxy-1-oxo-phenelenyl)ethylenediamine (62554-97-6)

Guidance literature:

With potassium hydroxide;

Reference yield:

N,N'-ethylenediphthalimide (607-26-1) → N,N'-bis(2-carboxy-1-oxo-phenelenyl)ethylenediamine (62554-97-6)

Guidance literature:

upstream raw materials:

N,N'-ethylenediphthalimide

phthalic anhydride

ethylenediamine

Refernces

• 1、 Garg, Bhagwan S.,Sharma, Rakesh K.,Kumar, Vinod,Reddy,Mittal, Sachin. "Synthesis and studies on metal coordination with a novel carboxyamide ligand". . p. 2789 - 2794. Retrieved 2002.