Technology Process of Nonacosane
There total 10 articles about Nonacosane which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
C22H41IrN2O2P2; Re2O7/Al2O3; 1,3,5-trimethyl-benzene;
at 175 ℃;
for 168h;
Inert atmosphere;
DOI:10.1002/adsc.200900539
- Guidance literature:
-
C43H72N4O4S2;
With
sodium tetrahydroborate;
In
methanol; dichloromethane;
at 0 - 20 ℃;
With
sodium hydroxide;
In
methanol; dichloromethane; water;
at 20 ℃;
for 24h;
DOI:10.1002/chem.202004946
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.5 h / -78 °C / Inert atmosphere
1.2: -78 - 20 °C / Inert atmosphere
2.1: benzophenone; N-hydroxyphthalimide / 48 h / 25 °C / Inert atmosphere; Sealed tube; Irradiation
3.1: ethanol / 24 h / 20 °C
4.1: sodium tetrahydroborate / dichloromethane; methanol / 0 - 20 °C
4.2: 24 h / 20 °C
With
sodium tetrahydroborate; benzophenone; N-hydroxyphthalimide; oxalyl dichloride; dimethyl sulfoxide;
In
methanol; ethanol; dichloromethane;
DOI:10.1002/chem.202004946
