Technology Process of 7-Methyl-3-methylene-1-octanol
There total 6 articles about 7-Methyl-3-methylene-1-octanol which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tetrabutyl ammonium fluoride;
In
tetrahydrofuran; benzene;
at 20 ℃;
for 2h;
Inert atmosphere;
Glovebox;
DOI:10.1021/jacs.7b08459
- Guidance literature:
-
Multi-step reaction with 2 steps
1: BH3 / tetrahydrofuran
2: (i) Ag2O, aq. NaOH, (ii) aq. H2O2
With
borane;
In
tetrahydrofuran;
DOI:10.1021/jo00864a019
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1H-imidazole / tetrahydrofuran / 20 °C / Inert atmosphere
2: palladium diacetate; caesium carbonate; 1-(diphenylphosphino)ferrocene-1-(di-tert-butylphosphino)ferrocene / benzene / 24 h / 20 °C / Inert atmosphere; Glovebox; Irradiation
3: tetrabutyl ammonium fluoride / tetrahydrofuran; benzene / 2 h / 20 °C / Inert atmosphere; Glovebox
With
1H-imidazole; 1-(diphenylphosphino)ferrocene-1-(di-tert-butylphosphino)ferrocene; tetrabutyl ammonium fluoride; palladium diacetate; caesium carbonate;
In
tetrahydrofuran; benzene;
DOI:10.1021/jacs.7b08459