Naphth[2,3-c]acridine-5,8,14(13H)-trione

Base Information

• Chemical Name: Naphth[2,3-c]acridine-5,8,14(13H)-trione
• CAS No.: 3569-01-5
• Molecular Formula: C21H11 N O3
• Molecular Weight: 325.323
• Hs Code.: 2933990090
• European Community (EC) Number: 222-665-8
• DSSTox Substance ID: DTXSID9063083
• Nikkaji Number: J216.208C
• Wikidata: Q81990466
• Mol file: 3569-01-5.mol

Synonyms:Naphth[2,3-c]acridine-5,8,14(13H)-trione;3569-01-5;13H-Naphtho[2,3-c]acridine-5,8,14-trione;Naphtho[2,3-c]acridine-5,8,14(13H)-trione;Naphth(2,3-c)acridine-5,8,14(13H)-trione;13H-NAPHTHO(2,3-C)ACRIDINE-5,8,14-TRIONE;SCHEMBL6825452;DTXSID9063083;EINECS 222-665-8;AKOS000592916;Naphtho[2,3-c]acridine-5,8,14(13H)-trione #

Chemical Property of Naphth[2,3-c]acridine-5,8,14(13H)-trione

Chemical Property:

• Vapor Pressure: 3.03E-14mmHg at 25°C
• Boiling Point: 597.6°Cat760mmHg
• PKA: -5.88±0.20(Predicted)
• Flash Point: 231.8°C
• PSA: 67.00000
• Density: 1.425g/cm³
• LogP: 3.45670
• XLogP3: 3.9
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 0
• Exact Mass: 325.07389321
• Heavy Atom Count: 25
• Complexity: 614

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C2C(=C1)C(=O)C3=C(C2=O)C4=C(C=C3)C(=O)C5=CC=CC=C5N4

Technology Process of Naphth[2,3-c]acridine-5,8,14(13H)-trione

There total 26 articles about Naphth[2,3-c]acridine-5,8,14(13H)-trione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-anilido-o-carboxy-9,10-anthracene-dione (19795-96-1) → 13H-Naphtho[2,3-c]acridine-5,8,14-trione (3569-01-5)

Guidance literature:

With sulfuric acid; at 100 - 110 ℃;

Reference yield:

1-anilino-9,10-dioxo-9,10-dihydro-anthracene-2-carbonyl chloride → 13H-Naphtho[2,3-c]acridine-5,8,14-trione (3569-01-5)

Guidance literature:

With aluminium trichloride; benzene;

Reference yield:

1-amino-2-benzoyl-anthraquinone (6337-19-5) → 13H-Naphtho[2,3-c]acridine-5,8,14-trione (3569-01-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 1) NaNO₂/H₂SO₄; 2) NaN₃ / 1) AcOH, 20-25 deg C, 15-20 min; 2) H₂O, 10-15 min

2: nitrobenzene / 7 h / Heating

With sodium azide; sulfuric acid; sodium nitrite; In nitrobenzene;

DOI:10.1007/BF00512807

upstream raw materials:

1-anilido-o-carboxy-9,10-anthracene-dione

1-anilino-9,10-dioxo-9,10-dihydro-anthracene-2-carboxylic acid

N-(9,10-dioxo-9,10-dihydro-[1]anthryl)-anthranilic acid methyl ester

1-chloroanthracene-9,10-dione

Downstream raw materials:

6,10,12-trichloro-13H-naphth[2,3-c]acridine-5,8,14-trione

9-oxo-9,10-dihydro-acridine-3-carboxylic acid

benzoic acid

Refernces