1,2-Dihydroxyphenanthrene

Base Information

• Chemical Name: 1,2-Dihydroxyphenanthrene
• CAS No.: 19551-04-3
• Molecular Formula: C14H10O2
• DSSTox Substance ID: DTXSID60429475
• Nikkaji Number: J82.875K
• Wikidata: Q27104405
• Metabolomics Workbench ID: 52188
• Mol file: 19551-04-3.mol

Synonyms:1,2-Dihydroxyphenanthrene;phenanthrene-1,2-diol;19551-04-3;1,2-Phenanthrenediol;dihydroxyphenanthrene;c0546;SCHEMBL888244;CHEBI:37452;DTXSID60429475;Q27104405

Chemical Property of 1,2-Dihydroxyphenanthrene

Chemical Property:

• XLogP3: 3.7
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 0
• Exact Mass: 210.068079557
• Heavy Atom Count: 16
• Complexity: 253

Purity/Quality:

99.90% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C2C(=C1)C=CC3=C2C=CC(=C3O)O

Technology Process of 1,2-Dihydroxyphenanthrene

There total 1 articles about 1,2-Dihydroxyphenanthrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

phenanthrene 1,2-quinone (573-12-6) → phenanthrene-1,2-diol (19551-04-3) + trans-1,2-dihydroxy-1,2-dihydrophenanthrene (60917-41-1,28622-66-4)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether; for 2h; Heating;

DOI:10.1021/jo01310a029

Reference yield: 63.0%

phenanthrene-1,2-diol (19551-04-3) → phenanthrene 1,2-quinone (573-12-6)

Guidance literature:

With iron(III) chloride; In hydrogenchloride;

DOI:10.1021/jo01310a029

Reference yield: 33.0%

phenanthrene-1,2-diol (19551-04-3) + acetic anhydride (108-24-7) → 1,2-Diacetoxy-phenanthren (19551-05-4)

Guidance literature:

In pyridine;

DOI:10.1021/jo01310a029

upstream raw materials:

phenanthrene 1,2-quinone

Downstream raw materials:

1,2-Diacetoxy-phenanthren

phenanthrene 1,2-quinone

Refernces