1,1-Dichlorodisilane

Base Information

• Chemical Name: 1,1-Dichlorodisilane
• CAS No.: 20424-84-4
• Molecular Formula: Cl2H4Si2
• Molecular Weight: 127.07700
• Mol file: 20424-84-4.mol

Synonyms:1,1-Dichlorodisilane;

Chemical Property of 1,1-Dichlorodisilane

Chemical Property:

• PSA: 0.00000
• LogP: 0.61740

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,1-Dichlorodisilane

There total 1 articles about 1,1-Dichlorodisilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

H3SiSiHCl(CF3SO3) (152644-89-8) + triethylamine hydrochloride (554-68-7) → 1,1-dichlorodisilane (20424-84-4)

Guidance literature:

In dibutyl ether; addn. of Et3NHCl to a soln. of H3SiSiHClCF3SO3 at -20°C under exclusion of air and moisture and stirring for 2 h; fractionating the chlorodisilane from the resulting soln. in vacuo at -20°C;

upstream raw materials:

H₃SiSiHCl(CF₃SO₃)

triethylamine hydrochloride