Technology Process of 4-DIMETHYLAMINOPHENYLAZOPHENYL-4'-MALEIM
There total 5 articles about 4-DIMETHYLAMINOPHENYLAZOPHENYL-4'-MALEIM which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C18H18N4O3;
With
triethylamine;
In
acetone;
at 60 ℃;
for 0.0833333h;
With
manganese(II) acetate; acetic anhydride;
at 60 ℃;
for 4h;
DOI:10.1039/c2jm32992a
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: hydrogenchloride; sodium nitrite / water / 1 h / Cooling with ice
1.2: 2 h / 0 - 5 °C
2.1: sodiumsulfide nonahydrate / 1,4-dioxane; water / 80 °C / Inert atmosphere
3.1: acetone / 8 h / 60 °C
4.1: triethylamine / acetone / 0.08 h / 60 °C
4.2: 4 h / 60 °C
With
hydrogenchloride; sodiumsulfide nonahydrate; triethylamine; sodium nitrite;
In
1,4-dioxane; water; acetone;
DOI:10.1039/c2jm32992a
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: hydrogenchloride; sodium nitrite / water / 1 h / Cooling with ice
1.2: 2 h / 0 - 5 °C
2.1: sodiumsulfide nonahydrate / 1,4-dioxane; water / 80 °C / Inert atmosphere
3.1: acetone / 8 h / 60 °C
4.1: triethylamine / acetone / 0.08 h / 60 °C
4.2: 4 h / 60 °C
With
hydrogenchloride; sodiumsulfide nonahydrate; triethylamine; sodium nitrite;
In
1,4-dioxane; water; acetone;
DOI:10.1039/c2jm32992a
