CYCLOHEXANONE PHENYLHYDRAZONE

Base Information

• Chemical Name: CYCLOHEXANONE PHENYLHYDRAZONE
• CAS No.: 946-82-7
• Molecular Formula: C12H16 N2
• Molecular Weight: 188.272
• Hs Code.: 2928000090
• Mol file: 946-82-7.mol

Synonyms:Cyclohexanone,phenylhydrazone (6CI,7CI,8CI,9CI); Phenylhydrazonocyclohexane

Chemical Property of CYCLOHEXANONE PHENYLHYDRAZONE

Chemical Property:

• Vapor Pressure: 0.000905mmHg at 25°C
• Boiling Point: 303.9°C at 760 mmHg
• Flash Point: 137.6°C
• PSA: 24.39000
• Density: 1.05g/cm³
• LogP: 3.49160

Purity/Quality:

99% ^*data from raw suppliers

Cyclohexanonephenylhydrazone ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of CYCLOHEXANONE PHENYLHYDRAZONE

There total 8 articles about CYCLOHEXANONE PHENYLHYDRAZONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

cyclohexanone (108-94-1,11119-77-0,9003-41-2,9075-99-4) + phenylhydrazine (100-63-0) → cyclohexanone phenylhydrazone (946-82-7)

Guidance literature:

DOI:10.1007/BF00522729

Reference yield: 92.0%

phenylhydrazine hydrochloride (59-88-1) + cyclohexanone (108-94-1,11119-77-0,9003-41-2,9075-99-4) → cyclohexanone phenylhydrazone (946-82-7)

Guidance literature:

With hydroxylamine hydrochloride; potassium carbonate; for 0.0166667h; microwave irradiation;

DOI:10.1071/CH05107

Reference yield: 38.0%

→ cyclohexanone phenylhydrazone (946-82-7)

Guidance literature:

With sodium methylate; In toluene; for 3h; Reflux; Dean-Stark;

upstream raw materials:

cyclohexanone

phenylhydrazine

cyclohexanethione

1-(methylthio)cyclohexene

Downstream raw materials:

acetic acid-(cyclohexylidene-phenyl-hydrazide)

1,2,3,4-tetrahydrocarbazole

N-phenyl-N'-(1-phenyl-cyclohexyl)-hydrazine

Phenyl-azo-cyclohexan

Refernces

• 1、 Zhang, Mo,Shang, Ze-Ren,Li, Xiao-Tang,Zhang, Jia-Nan,Wang, Yong,Li, Kang,Li, Yang-Yang,Zhang, Zhan-Hui. "Simple and efficient approach for synthesis of hydrazones from carbonyl compounds and hydrazides catalyzed by meglumine". . p. 178 - 187. Retrieved 2017/01/10.
• 2、 Liu, Pengyuan,Forni, Amanda,Chen, Hao. "Development of solvent-free ambient mass spectrometry for green chemistry applications". . p. 4024 - 4032. Retrieved 2014/05/06.