2H-Cycloheptoxazole-2-thione

Base Information

• Chemical Name: 2H-Cycloheptoxazole-2-thione
• CAS No.: 225112-78-7
• Molecular Formula: C8H5NOS
• Mol file: 225112-78-7.mol

Synonyms:

Chemical Property of 2H-Cycloheptoxazole-2-thione

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2H-Cycloheptoxazole-2-thione

There total 1 articles about 2H-Cycloheptoxazole-2-thione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

carbon disulfide (75-15-0,12122-00-8) + 2-aminotropone (6264-93-3) → 2H-Cycloheptaoxazole-2-thione (225112-78-7) + 1-thia-3-azaazulene-2(1H)-one (25946-69-4)

Guidance literature:

With potassium tert-butylate; In dichloromethane; at 0 ℃; for 2h;

DOI:10.3987/com-01-9322

Reference yield: 33.0%

2H-Cycloheptaoxazole-2-thione (225112-78-7) → 1-thia-3-azaazulene-2(1H)-one (25946-69-4)

Guidance literature:

With hydrogenchloride; at 20 ℃; for 6h;

DOI:10.3987/com-01-9322

upstream raw materials:

carbon disulfide

2-aminotropone

Downstream raw materials:

1-thia-3-azaazulene-2(1H)-one

Refernces