4-((4-Aminophenyl)azo)-5-methyl-2-methoxyaniline

Base Information

• Chemical Name: 4-((4-Aminophenyl)azo)-5-methyl-2-methoxyaniline
• CAS No.: 6232-57-1
• Molecular Formula: C14H16N4O
• Molecular Weight: 256.307
• Hs Code.: 2927000090
• European Community (EC) Number: 228-341-2
• DSSTox Substance ID: DTXSID7064152
• Nikkaji Number: J33.591F
• Mol file: 6232-57-1.mol

Synonyms:Disperse Diazo Black 3BF;6232-57-1;4-((4-Aminophenyl)azo)-5-methyl-2-methoxyaniline;C.I. Disperse Black 2;Fast Black C Base;4,4'-Diamino-3-methoxy-6-methylazobenzene;4-[(4-aminophenyl)diazenyl]-2-methoxy-5-methylaniline;EINECS 228-341-2;4-[2-(4-aminophenyl)diazen-1-yl]-2-methoxy-5-methylaniline;C.I. 11255;Benzenamine, 4-((4-aminophenyl)azo)-2-methoxy-5-methyl-;Benzenamine, 4-(2-(4-aminophenyl)diazenyl)-2-methoxy-5-methyl-;4-((4-Aminophenyl)azo)-5-methyl-o-anisidine;4-[(4-AMINOPHENYL)AZO]-5-METHYL-O-ANISIDINE;4-((4-Aminophenyl)diazenyl)-2-methoxy-5-methylaniline;Benzenamine, 4-[(4-aminophenyl)azo]-2-methoxy-5-methyl-;SCHEMBL2027081;DTXSID7064152;MFCD00059857;AKOS024340813;C.I.11255;CS-0454335;D1615;D89893;4,4'-DIAMINO-5-METHOXY-2-METHYLAZOBENZENE

Chemical Property of 4-((4-Aminophenyl)azo)-5-methyl-2-methoxyaniline

Chemical Property:

• Vapor Pressure: 1.89E-09mmHg at 25°C
• Refractive Index: 1.615
• Boiling Point: 482 °C at 760 mmHg
• PKA: 3.47±0.10(Predicted)
• Flash Point: 245.3 °C
• PSA: 85.99000
• Density: 1.22 g/cm³
• LogP: 4.74580
• Storage Temp.: Refrigerator
• Solubility.: DMSO (Slightly), Methanol (Slightly)
• XLogP3: 2.7
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 3
• Exact Mass: 256.13241115
• Heavy Atom Count: 19
• Complexity: 302

Purity/Quality:

98%,99%, ^*data from raw suppliers

Disperse Diazo Black 3BF ^*data from reagent suppliers

Safty Information:

• Statements: 20/21/22
• Safety Statements: 22-36/37/39

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Canonical SMILES: CC1=CC(=C(C=C1N=NC2=CC=C(C=C2)N)OC)N

Technology Process of 4-((4-Aminophenyl)azo)-5-methyl-2-methoxyaniline

There total 1 articles about 4-((4-Aminophenyl)azo)-5-methyl-2-methoxyaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

p-nitrobenzenediazonium (14368-49-1) + Cresidine (120-71-8) → (4-amino-5-methoxy-2-methyl-phenyl)-(4-amino-phenyl)-diazene (6232-57-1)

Guidance literature:

und Reduzieren des Reaktionsprodukts;

Reference yield:

(4-amino-5-methoxy-2-methyl-phenyl)-(4-amino-phenyl)-diazene (6232-57-1) → C52H54N6O7 (80793-40-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) diazotization, 2.) azocoupling

Reference yield:

(4-amino-5-methoxy-2-methyl-phenyl)-(4-amino-phenyl)-diazene (6232-57-1) + 3-methyl-phenol (108-39-4) → C28H26N6O3 (80793-49-3)

Guidance literature:

Multistep reaction; 1.) diazotization, 2.) azocoupling;

upstream raw materials:

p-nitrobenzenediazonium

Cresidine

Downstream raw materials:

C₂₈H₂₆N₆O₃

C₅₂H₅₄N₆O₇