Technology Process of 1-Hepten-3-ol, 3-methyl-
There total 1 articles about 1-Hepten-3-ol, 3-methyl- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
dichloro(N,N,N’,N‘-tetramethylethylenediamine)zinc;
In
tetrahydrofuran; diethyl ether;
at 0 ℃;
for 0.5h;
Product distribution;
other α,β-unsaturated ketones, other Grignard reagents;
DOI:10.1021/jo00371a015
- Guidance literature:
-
With
pyridine; xanth-9-one; bis(2,4-acetylacetonate)cobalt(II); hydrogen;
In
tetrahydrofuran;
under 760 Torr;
Ambient temperature;
Irradiation;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 87.6 percent / 47percent hydrobromic acid / 1 h / 0 - 10 °C
2: 83.3 percent / EtONa / ethanol; benzene / 1.) 1 h, 2.) reflux, 1 h
3: 71.8 percent / barium hydroxide octahydrate / aq. ethanol / Heating
4: 1.) Mg / 1.) THF, 2.) reflux, 1 h
5: 77.5 percent / 47percent hydrobromic acid / 1 h / 0 - 10 °C
6: 48.2 percent / KOH / dimethylformamide / 1.) 1 h, 2.) r.t., overnight
7: m-chloroperbenzoic acid / CH2Cl2 / 2 h
With
potassium hydroxide; barium hydroxide octahydrate; hydrogen bromide; sodium ethanolate; magnesium; 3-chloro-benzenecarboperoxoic acid;
In
ethanol; dichloromethane; N,N-dimethyl-formamide; benzene;