Diazene, bis(4-butoxyphenyl)-, 1-oxide

Base Information

• Chemical Name: Diazene, bis(4-butoxyphenyl)-, 1-oxide
• CAS No.: 17051-01-3
• Molecular Formula: C₂₀H₂₆N₂O₃
• Molecular Weight: 342.438
• Hs Code.: 2927000090
• Mol file: 17051-01-3.mol

Synonyms:4,4'-Dibutoxyazoxybenzene;17051-01-3;Diazene, bis(4-butoxyphenyl)-, 1-oxide;4,4'-Di-N-butoxyazoxybenzene;(4-butoxyphenyl)-(4-butoxyphenyl)imino-oxidoazanium;Azoxy-bis-(p-n-butoxybenzene);SCHEMBL19460318;AKOS015839669;(Z)-1,2-bis(4-butoxyphenyl)diazene oxide;D1096;FT-0728176;T70409;(NZ,Z)-4-butoxy-N-[(4-butoxyphenyl)imino]benzen-1-imine oxide

Chemical Property of Diazene, bis(4-butoxyphenyl)-, 1-oxide

Chemical Property:

• Vapor Pressure: 4.04E-09mmHg at 25°C
• Boiling Point: 485.8°Cat760mmHg
• Flash Point: 247.6°C
• PSA: 59.57000
• Density: 1.06g/cm³
• LogP: 6.49330
• XLogP3: 5.6
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 10
• Exact Mass: 342.19434270
• Heavy Atom Count: 25
• Complexity: 373

Purity/Quality:

98%,99%, ^*data from raw suppliers

4,4'-Dibutoxyazoxybenzene ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: CCCCOC1=CC=C(C=C1)N=[N+](C2=CC=C(C=C2)OCCCC)[O-]

Technology Process of Diazene, bis(4-butoxyphenyl)-, 1-oxide

There total 6 articles about Diazene, bis(4-butoxyphenyl)-, 1-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

1-butoxy-4-nitrobenzene (7244-78-2) → 4,4'-di-n-butyloxyazoxybenzene (17051-01-3,113787-54-5)

Guidance literature:

With bismuth; at 20 ℃; for 3h;

DOI:10.1021/jo0203645

Reference yield:

4-nitro-phenol (100-02-7,78813-13-5,89830-32-0) → 4,4'-di-n-butyloxyazoxybenzene (17051-01-3,113787-54-5)

Guidance literature:

Multi-step reaction with 2 steps

1: K₂CO₃ / dimethylformamide

2: 91 percent / bismuth / 3 h / 20 °C

With bismuth; potassium carbonate; In N,N-dimethyl-formamide;

DOI:10.1021/jo0203645

Reference yield:

1-butoxy-4-nitrobenzene (7244-78-2) → 4,4'-dibutoxy azoxy benzene (17051-01-3,113787-54-5)

Guidance literature:

With ethanol; sodium acetate; Reduktion an einer Blei-Kathode;

upstream raw materials:

1-butoxy-4-nitrobenzene

4-nitro-phenol

potassium 4-nitrophenolate

Refernces