2,2'-DIHYDROXYDIPHENYL ETHER

Base Information

• Chemical Name: 2,2'-DIHYDROXYDIPHENYL ETHER
• CAS No.: 15764-52-0
• Molecular Formula: C12H10 O3
• Molecular Weight: 202.21
• Hs Code.: 2907299090
• Mol file: 15764-52-0.mol

Synonyms:Phenol,2,2'-oxydi- (7CI,8CI); 2,2'-Dihydroxydiphenyl ether; 2,2'-Oxybisphenol;2,2'-Oxydiphenol; PD 048890; o-Hydroxyphenyl ether

Chemical Property of 2,2'-DIHYDROXYDIPHENYL ETHER

Chemical Property:

• Melting Point: 123°C
• Boiling Point: 299.3°Cat760mmHg
• Flash Point: 134.8°C
• PSA: 49.69000
• Density: 1.288g/cm³
• LogP: 2.89010
• Storage Temp.: Sealed in dry,Room Temperature
• Solubility.: very faint turbidity in Methanol

Purity/Quality:

98%,99%, ^*data from raw suppliers

2,2'-Dihydroxydiphenyl Ether ^*data from reagent suppliers

Safty Information:

• Statements: 36/37/38
• Safety Statements: 26-36/37/39

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,2'-DIHYDROXYDIPHENYL ETHER

There total 9 articles about 2,2'-DIHYDROXYDIPHENYL ETHER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.6%

benzene-1,2-diol (120-80-9,19481-10-8,37349-32-9) → 2,2'-oxydiphenol (15764-52-0)

Guidance literature:

With Diethyl carbonate; at 200 ℃; for 5h; Temperature;

Reference yield: 94.0%

di(2-methoxyphenyl) ether (1655-70-5) → 2,2'-oxydiphenol (15764-52-0)

Guidance literature:

With boron tribromide; In dichloromethane; at 0 ℃; for 3h;

DOI:10.1021/jo00003a055

Reference yield: 80.0%

diphenylether (101-84-8) → 2,2'-oxydiphenol (15764-52-0)

Guidance literature:

diphenylether; With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In tetrahydrofuran;

With Trimethyl borate; In tetrahydrofuran;

With dihydrogen peroxide; potassium hydroxide; In tetrahydrofuran;

DOI:10.1021/acs.inorgchem.5b02288

upstream raw materials:

di(2-methoxyphenyl) ether

tetra(n-butyl)ammonium hydrogensulfate

potassium carbonate

benzene-1,2-diol

Downstream raw materials:

dioxin

2,2'-dihydroxy-5,5'-dibromodiphenyl ether

6,6′-dihydroxy-2,2′,4,4′-tetrabromodiphenyl ether

Oxybis(2,1-phenylenoxy-N,N-dicyclohexylacetamid)

Refernces

• 1、 Torizuka,Sato. "". . p. 190,192,193. Retrieved 1979.
• 2、 Andrews, Ryan J.,Cano, Maria T.,Carta, Veronica,MacLachlan, Mark J.,Patrick, Brian O.,Soto, Miguel A.. "Multiresponsive Cyclometalated Crown Ether Bearing a Platinum(II) Metal Center". supporting information. p. 2999 - 3006. Retrieved 2021/12/06.