Technology Process of 2-Propenoic acid, 2-azido-, phenylmethyl ester
There total 2 articles about 2-Propenoic acid, 2-azido-, phenylmethyl ester which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium azide;
In
N,N-dimethyl-formamide;
at 65 ℃;
for 0.133333h;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 98 percent / Br2 / CH2Cl2
2: 95 percent / NaN3 / dimethylformamide / 0.13 h / 65 °C
With
sodium azide; bromine;
In
dichloromethane; N,N-dimethyl-formamide;
1: Bromination / 2: Elimination;
- Guidance literature:
-
2-azidoacrylic acid benzyl ester;
In
toluene;
at 110 ℃;
furan;
In
toluene;
at 20 ℃;
for 168h;
Further stages.;
DOI:10.1039/b106985n
