2,6-Diacetylpyridine

Base Information Edit

Chemical Name:2,6-Diacetylpyridine
CAS No.:1129-30-2
Molecular Formula:C9H9NO2
Molecular Weight:163.176
Hs Code.:29333990
European Community (EC) Number:214-442-9
NSC Number:63355
UNII:P34UXL3MYV
DSSTox Substance ID:DTXSID10150202
Nikkaji Number:J149.829K
Wikipedia:2,6-Diacetylpyridine
Wikidata:Q4596808
Mol file:1129-30-2.mol

Synonyms:2,6-Diacetylpyridine;1129-30-2;1-(6-acetylpyridin-2-yl)ethanone;1,1'-(pyridine-2,6-diyl)diethanone;Pyridine-2,6-diacetyl;MFCD00006304;Ethanone, 1,1'-(2,6-pyridinediyl)bis-;P34UXL3MYV;1-(6-acetylpyridin-2-yl)ethan-1-one;EINECS 214-442-9;NSC-63355;1,1'-(2,6-Pyridinediyl)bis[ethanone];1,1'-(2,6-PYRIDINEDIYL)BIS(ETHANONE);1-(6-Acetyl-pyridin-2-yl)-ethanone;NSC63355;2,6diacetylpyridine;UNII-P34UXL3MYV;2 pound not6-Diacetylpyridine;2,6-Diacetylpyridine, 99%;SCHEMBL455687;BEZVGIHGZPLGBL-UHFFFAOYSA-;DTXSID10150202;1,1'-pyridine-2,6-diyldiethanone;AMY14457;BBL100152;GEO-00906;NSC 63355;STK087382;AKOS003595902;AC-6429;CS-W001999;NCGC00340769-01;BP-20094;SY010398;TS-03571;D2377;FT-0610526;D58390;2,6-Diacetylpyridine, purum, >=98.0% (GC);AB01332223-02;EN300-6736941;Q4596808;W-108632

Suppliers and Price of 2,6-Diacetylpyridine

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
2,6-Diacetylpyridine
50mg
$ 60.00

TCI Chemical
2,6-Diacetylpyridine >98.0%(GC)
25g
$ 397.00

TCI Chemical
2,6-Diacetylpyridine >98.0%(GC)
5g
$ 120.00

SynQuest Laboratories
2,6-Diacetylpyridine 98%
5 g
$ 115.00

SynQuest Laboratories
2,6-Diacetylpyridine 98%
25 g
$ 300.00

Sigma-Aldrich
2,6-Diacetylpyridine 99%
25g
$ 320.00

Sigma-Aldrich
2,6-Diacetylpyridine 99%
1g
$ 35.00

Sigma-Aldrich
2,6-Diacetylpyridine 99%
5g
$ 116.00

Matrix Scientific
2,6-Diacetylpyridine 97%
5g
$ 65.00

Matrix Scientific
2,6-Diacetylpyridine 97%
1g
$ 15.00

Total 152 raw suppliers

Chemical Property of 2,6-Diacetylpyridine Edit

Chemical Property:

Appearance/Colour:white to off-white crystalline needles or powder
Vapor Pressure:0.00251mmHg at 25°C
Melting Point:79-82 °C
Refractive Index:1.521
Boiling Point:287.2 °C at 760 mmHg
PKA:0.88±0.10(Predicted)
Flash Point:131.9 °C
PSA：47.03000
Density:1.119 g/cm³
LogP:1.48680
Storage Temp.:Inert atmosphere,Room Temperature
Water Solubility.:Soluble in water, chloroform, and DMSO.
XLogP3:0.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:163.063328530
Heavy Atom Count:12
Complexity:181

Purity/Quality:

99% ^*data from raw suppliers

2,6-Diacetylpyridine ^*data from reagent suppliers

Safty Information:

Pictogram(s): Xi,F
Hazard Codes:Xi,F
Statements: 36/37/38-15-10
Safety Statements: 26-36-43-7/8

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

Chemical Classes:Nitrogen Compounds -> Pyridines
Canonical SMILES:CC(=O)C1=NC(=CC=C1)C(=O)C
Uses 2,6-Diacetylpyridine is used as intermediate in organic synthesis. It is a precursor to ligands in coordination chemistry.

Technology Process of 2,6-Diacetylpyridine

There total 12 articles about 2,6-Diacetylpyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 3739-94-4
2,6-Pyridinedicarbonyl dichloride

: 917-54-4
methyllithium

: 1129-30-2
2,6-Diacetylpyridine

Guidance literature:: With copper(l) iodide; In tetrahydrofuran; at -78 ℃;
DOI:10.1016/0040-4039(95)02298-8

Reference yield: 88.0%

: 36763-33-4
N²,N²,N⁶,N⁶-tetraethyl-2,6-pyridinedicarboxamide

: 676-58-4
methylmagnesium chloride

: 1129-30-2
2,6-Diacetylpyridine

Guidance literature:: N²,N²,N⁶,N⁶-tetraethyl-2,6-pyridinedicarboxamide; methylmagnesium chloride; In tetrahydrofuran; at 0 - 20 ℃; for 3h;

With hydrogenchloride; In tetrahydrofuran; water; at 0 ℃;
DOI:10.1016/j.tetlet.2012.11.004

Reference yield: 65.0%

: 15658-60-3
diethyl-2,6-pyridinedicarbonyl ester

: 1129-30-2
2,6-Diacetylpyridine

Guidance literature:: diethyl-2,6-pyridinedicarbonyl ester; With sodium ethanolate; In ethyl acetate; for 20h; Reflux;

With hydrogenchloride; In ethyl acetate; at 0 ℃; for 20h; Reflux;