2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-Pentadecafluorooctanal

Base Information

• Chemical Name: 2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-Pentadecafluorooctanal
• CAS No.: 335-60-4
• Molecular Formula: C₈HF₁₅O
• Molecular Weight: 398.071
• Hs Code.: 2913000090
• Mol file: 335-60-4.mol

Synonyms:Pentadecafluor-octanal;Octanal,pentadecafluoro;pentadecafluoro-octanal;Octanal, pentadecafluoro-;

Chemical Property of 2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-Pentadecafluorooctanal

Chemical Property:

• PSA: 17.07000
• LogP: 4.55940

Purity/Quality:

PENTADECAFLUORO-OCTANAL 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-Pentadecafluorooctanal

There total 3 articles about 2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-Pentadecafluorooctanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

{1-[Dimethyl-(1,1,2-trimethyl-propyl)-silanyloxy]-2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-pentadecafluoro-octyl}-dimethyl-amine → pentadecafluoro-octanal (335-60-4)

Guidance literature:

With sulfuric acid; at 90 ℃;

DOI:10.1002/hlca.19880710210

Reference yield:

→ pentadecafluoro-octanal (335-60-4)

Guidance literature:

With lithium aluminium tetrahydride; diethyl ether; at -70 ℃;

DOI:10.1021/ja01630a097

Reference yield:

perfluoroheptyl iodide (335-58-0) → pentadecafluoro-octanal (335-60-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 80 percent / Zn / 2 h / 0 - 5 °C

2: 75 percent / cc.H₂SO₄ / 90 °C

With sulfuric acid; zinc;

DOI:10.1002/hlca.19880710210

upstream raw materials:

perfluoroheptyl iodide

Downstream raw materials:

2,2,3,3,4,4,5,5,6,6,7,7,8,8,8-Pentadecafluoro-1-pentafluorophenyl-octan-1-one

2,3,5,6-Tetrafluoro-4-heptadecafluorooctyl-benzenethiol

Perfluor-n-octylbenzol

Ethyl E-3-F-heptyl 2-propenoate

Refernces

• 1、 Lang, Robert Werner. "Fluorine-Containing Organozinc Reagents. Part III. A New Formylation Reaction of Fluoroalkylzinc Halides". . p. 369 - 373. Retrieved 1988.