Technology Process of 4-Hexenoic acid,
6-(1,4-dihydro-3-methyl-1,4-dioxo-2-naphthalenyl)-4-methyl-, (E)-
There total 22 articles about 4-Hexenoic acid,
6-(1,4-dihydro-3-methyl-1,4-dioxo-2-naphthalenyl)-4-methyl-, (E)- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
oxone;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 2.5h;
Inert atmosphere;
DOI:10.1055/s-0034-1380002
- Guidance literature:
-
With
water; potassium hydroxide;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: potassium tert-butylate / tetrahydrofuran / 4 - 20 °C / Inert atmosphere
2: dodecyltrimethylammonium bromide / acetic acid / 1.5 h / 90 °C / Inert atmosphere
3: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 4 - 20 °C / Inert atmosphere
4: periodic acid / water; tetrahydrofuran-d8 / 1 h / 20 °C / Inert atmosphere
5: oxone / N,N-dimethyl-formamide / 2.5 h / 20 °C / Inert atmosphere
With
oxone; potassium tert-butylate; dodecyltrimethylammonium bromide; periodic acid; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; tetrahydrofuran-d8; dichloromethane; water; acetic acid; N,N-dimethyl-formamide;
DOI:10.1055/s-0034-1380002
