Technology Process of Carbonic acid, 1,1-dimethylethyl 2-iodophenyl ester
There total 1 articles about Carbonic acid, 1,1-dimethylethyl 2-iodophenyl ester which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
2-Iodophenol;
With
sodium hydride;
In
tetrahydrofuran;
at 0 - 20 ℃;
for 1h;
Inert atmosphere;
di-tert-butyl dicarbonate;
In
tetrahydrofuran;
at 0 - 20 ℃;
Inert atmosphere;
DOI:10.1016/j.tet.2014.03.073
- Guidance literature:
-
With
copper(l) iodide; triethylamine; triphenylphosphine;
palladium diacetate;
at 70 ℃;
for 6h;
DOI:10.1002/chem.200305284
- Guidance literature:
-
With
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine;
at 23 ℃;
for 20h;
Inert atmosphere;
DOI:10.1021/acs.orglett.9b03557
