Technology Process of Benzenepropanol, 3-fluoro-2-methyl-, methanesulfonate
There total 3 articles about Benzenepropanol, 3-fluoro-2-methyl-, methanesulfonate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: hydrogen / palladium hydroxide/carbon / ethanol / 22 h
2: lithium aluminium tetrahydride / tetrahydrofuran / 1.17 h / 0 °C
3: triethylamine / tetrahydrofuran / 0.17 h / 0 °C
With
lithium aluminium tetrahydride; hydrogen; triethylamine;
palladium hydroxide/carbon;
In
tetrahydrofuran; ethanol;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: piperidine / toluene / 22 h / Heating / reflux
2: hydrogen / palladium hydroxide/carbon / ethanol / 22 h
3: lithium aluminium tetrahydride / tetrahydrofuran / 1.17 h / 0 °C
4: triethylamine / tetrahydrofuran / 0.17 h / 0 °C
With
piperidine; lithium aluminium tetrahydride; hydrogen; triethylamine;
palladium hydroxide/carbon;
In
tetrahydrofuran; ethanol; toluene;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: lithium aluminium tetrahydride / tetrahydrofuran / 1.17 h / 0 °C
2: triethylamine / tetrahydrofuran / 0.17 h / 0 °C
With
lithium aluminium tetrahydride; triethylamine;
In
tetrahydrofuran;
