Technology Process of Phosphine oxide, tris(3,5-dimethylphenyl)-
There total 2 articles about Phosphine oxide, tris(3,5-dimethylphenyl)- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
dihydrogen peroxide;
In
tetrahydrofuran; water;
at 20 ℃;
for 2h;
DOI:10.1002/anie.201809275
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: Mg / tetrahydrofuran / 1 h / Heating
1.2: PCl3 / diethyl ether / 20 h / 20 °C
2.1: H2O2 / CH2Cl2
With
dihydrogen peroxide; magnesium;
In
tetrahydrofuran; dichloromethane;
DOI:10.1016/S0040-4039(03)00940-7
- Guidance literature:
-
With
2,6-dimethylpyridine; oxalyl dichloride; hydrogen; tris(2,6-difluorophenyl)borane triethylphosphine oxide;
In
(2)H8-toluene;
at 130 ℃;
for 2h;
under 3000.3 Torr;
Reagent/catalyst;
DOI:10.1002/anie.201809275