1-Bromo-3-n-hexylbenzene, 97+%

Base Information

• Chemical Name: 1-Bromo-3-n-hexylbenzene, 97+%
• CAS No.: 38409-59-5
• Molecular Formula: C12H17Br
• Molecular Weight: 241.171
• Hs Code.: 2903999090
• Mol file: 38409-59-5.mol

Synonyms:1-Bromo-3-hexylbenzene;1-Bromo-3-n-hexylbenzene;3-(n-Hexyl)bromobenzene;

Chemical Property of 1-Bromo-3-n-hexylbenzene, 97+%

Chemical Property:

• Vapor Pressure: 0.00674mmHg at 25°C
• Refractive Index: 1.518
• Boiling Point: 279.6 °C at 760 mmHg
• Flash Point: 144.7 °C
• PSA: 0.00000
• Density: 1.179 g/cm³
• LogP: 4.57190
• Water Solubility.: Insoluble in water. Fully miscible with ethanol, acetone, toluene, methylene chloride.

Purity/Quality:

98%,99%, ^*data from raw suppliers

1-Bromo-3-hexylbenzene ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: 1-Bromo-3-n-hexylbenzene is used as intermediates in pharmaceutical industry.

Technology Process of 1-Bromo-3-n-hexylbenzene, 97+%

There total 2 articles about 1-Bromo-3-n-hexylbenzene, 97+% which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

1-bromo-hexane (111-25-1) + 1,3-dibromobenzene (108-36-1) → 1-bromo-3-hexylbenzene (38409-59-5)

Guidance literature:

1,3-dibromobenzene; With n-butyllithium; In tetrahydrofuran; at -60 ℃; for 2h; Inert atmosphere;

1-bromo-hexane; In tetrahydrofuran; at -10 ℃; for 6h; Inert atmosphere;

Reference yield:

→ 1-bromo-3-hexylbenzene (38409-59-5)

Guidance literature:

3-Amino-1-hexylbenzol;

Reference yield: 82.0%

2,2',3,3',5,5',6,6'-octafluoro-1,1'-biphenyl (3883-86-1) + 1-bromo-3-hexylbenzene (38409-59-5) → 1,4’-bis(3-hexylphenyl)-2′,2″,3′,3″,5′,5″,6′,6″-octafluorobiphenyl

Guidance literature:

With 7,7-dimethyloctanoic acid; palladium diacetate; tricyclohexylphosphine tetrafluoroborate; sodium t-butanolate; In water; toluene; at 130 ℃; for 24h; Sealed tube;

DOI:10.3390/molecules25163717

upstream raw materials:

1-bromo-hexane

1,3-dibromobenzene

Refernces