10-Chloro-9-anthraldehyde

Base Information

• Chemical Name: 10-Chloro-9-anthraldehyde
• CAS No.: 10527-16-9
• Molecular Formula: C15H9 Cl O
• Molecular Weight: 240.689
• Hs Code.: 2913000090
• European Community (EC) Number: 234-086-8
• UNII: 7RQ1N54G12
• DSSTox Substance ID: DTXSID8049202
• Nikkaji Number: J212.460B
• Wikidata: Q27268766
• ChEMBL ID: CHEMBL3187654
• Mol file: 10527-16-9.mol

Synonyms:10-Chloro-9-anthraldehyde;10-Chloroanthracene-9-carbaldehyde;10527-16-9;10-Chloro-9-anthracenecarbaldehyde;C15H9ClO;9-chloro-10-formylanthracene;UNII-7RQ1N54G12;9-Anthraldehyde, 10-chloro-;DTXSID8049202;7RQ1N54G12;EINECS 234-086-8;10-chloroanthracene-9-carboxaldehyde;C15-H9-Cl-O;SCHEMBL1616239;CHEMBL3187654;DTXCID3028473;10-Chloro-9-anthraldehyde, 97%;10 -chloroanthracene-9-carbaldehyde;10-chloro-anthracene-9-carbaldehyde;Tox21_202962;MFCD00001255;10-Chloro-9-anthracenecarbaldehyde #;AKOS003617823;9-Anthracenecarboxaldehyde, 10-chloro-;NCGC00260508-01;BS-49363;CAS-10527-16-9;CS-0237471;FT-0636728;EN300-18414;D97408;A801185;J-001377;Q27268766;Z57902299

Chemical Property of 10-Chloro-9-anthraldehyde

Chemical Property:

• Vapor Pressure: 8.46E-08mmHg at 25°C
• Melting Point: 215-218 °C(lit.)
• Boiling Point: 435.9°Cat760mmHg
• Flash Point: 221.8°C
• PSA: 17.07000
• Density: 1.327g/cm³
• LogP: 4.45890
• XLogP3: 4.5
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 1
• Exact Mass: 240.0341926
• Heavy Atom Count: 17
• Complexity: 267

Purity/Quality:

98%,99%, ^*data from raw suppliers

10-Chloro-9-anthraldehyde ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Chemical Classes: Other Classes -> Polycyclic Aromatic Hydrocarbons
• Canonical SMILES: C1=CC=C2C(=C1)C(=C3C=CC=CC3=C2Cl)C=O
• Uses: 10-Chloro-9-anthraldehyde was used in the preparation of trans-1-(10-methyl-9-anthryl)-2-(4-pyridyl)-ethene, 1-(10-chloro-9-anthryl)-2-(4-pyridyl)-ethene, 1-(10-methyl-9-anthryl)-2-(4-(N-methyl)-pyridinium)ethene iodide and 1-(10-chloro-9-anthryl)-2-(4-(N-methyl)pyridinium)ethene iodide.

Technology Process of 10-Chloro-9-anthraldehyde

There total 9 articles about 10-Chloro-9-anthraldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

10-chloro-9-anthracenemethanol (19996-02-2) → 10-chloro-9-anthraldehyde (10527-16-9)

Guidance literature:

With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In neat (no solvent); at 20 ℃; for 3h; Milling;

DOI:10.1039/c4ra00415a

Reference yield: 89.0%

9-anthracene aldehyde (642-31-9) → 10-chloro-9-anthraldehyde (10527-16-9)

Guidance literature:

With sulfuryl dichloride; In chlorobenzene; at 24.9 ℃;

DOI:10.1039/P29860000981

Reference yield: 80.0%

anthracen-9(10H)-one (90-44-8) + N,N-dimethyl-formamide (68-12-2,33513-42-7) → 10-chloro-9-anthraldehyde (10527-16-9)

Guidance literature:

With trichlorophosphate; for 0.0833333h; Microwave irradiation;

upstream raw materials:

anthracen-9(10H)-one

N-(4-methylphenyl)formamide

diphenylformamide

p-nitroformanilide

Downstream raw materials:

9,10-phenanthrenequinone

Refernces

• 1、 Achar, Tapas Kumar,Maiti, Saikat,Mal, Prasenjit. "IBX works efficiently under solvent free conditions in ball milling". . p. 12834 - 12839. Retrieved 2014/04/03.
• 2、 -. "Process for nucleophilic fluoroalkylation of aldehydes". . . Retrieved 2008/06/13.